cis-iodo-diphenylphosphine-tetracarbonyl-rhenium

Base Information

• Chemical Name: cis-iodo-diphenylphosphine-tetracarbonyl-rhenium
• CAS No.: 38427-21-3
• Molecular Formula: C₁₆H₁₁IO₄PRe
• Molecular Weight: 611.346

Synonyms:

Chemical Property of cis-iodo-diphenylphosphine-tetracarbonyl-rhenium

Chemical Property:

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Technology Process of cis-iodo-diphenylphosphine-tetracarbonyl-rhenium

There total 1 articles about cis-iodo-diphenylphosphine-tetracarbonyl-rhenium which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 5.0%

octacarbonyl-bis(μ-diphenylphosphido)-dirhenium + indium(III) iodide (13510-35-5) → C62H46IO8P5Re4 + (Re2(P(C6H5)2)2(CO)6(In(H2O)I2)2) + cis-iodo-diphenylphosphine-tetracarbonyl-rhenium (38427-21-3) + di-μ-iodo-μ-tetraphenyldiphosphaneoxide-bis(tricarbonyl-rhenium) + μ3-hydrido-μ3-iodo-tri-μ-diphenylphosphido-hexacarbonyl-triangulo-trirhenium

Guidance literature:

In xylene; reaction of the starting materials in dry xylene in a sealed glass tube at 220°C for 20 h, pptn.; centrifugation, ppt. is washed (CH2Cl2), identified by XRD as Re-In compd., elem.anal., centrifugate is chromd.(CHCl3/n-hexane) after evapn. of solvent, XRD, NMR-spectroscopy, elem. anal.;

upstream raw materials:

indium(III) iodide

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