3-Oxa-5,9,13-triazahexadecan-16-oic acid, 2,2,10-trimethyl-7-(1-methylethyl)-15-(2-methylpropyl)-4,8,12-trioxo-, phenylmethyl ester, (7S,10S,15S)-

Base Information

Chemical Name:3-Oxa-5,9,13-triazahexadecan-16-oic acid, 2,2,10-trimethyl-7-(1-methylethyl)-15-(2-methylpropyl)-4,8,12-trioxo-, phenylmethyl ester, (7S,10S,15S)-
CAS No.:200400-98-2
Molecular Formula:C29H47N3O6
Molecular Weight:533.709
Hs Code.:

3-Oxa-5,9,13-triazahexadecan-16-oic acid,
2,2,10-trimethyl-7-(1-methylethyl)-15-(2-methylpropyl)-4,8,12-trioxo-,
phenylmethyl ester, (7S,10S,15S)-

Synonyms:

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Chemical Property of 3-Oxa-5,9,13-triazahexadecan-16-oic acid, 2,2,10-trimethyl-7-(1-methylethyl)-15-(2-methylpropyl)-4,8,12-trioxo-, phenylmethyl ester, (7S,10S,15S)-

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Technology Process of 3-Oxa-5,9,13-triazahexadecan-16-oic acid, 2,2,10-trimethyl-7-(1-methylethyl)-15-(2-methylpropyl)-4,8,12-trioxo-, phenylmethyl ester, (7S,10S,15S)-

There total 3 articles about 3-Oxa-5,9,13-triazahexadecan-16-oic acid, 2,2,10-trimethyl-7-(1-methylethyl)-15-(2-methylpropyl)-4,8,12-trioxo-, phenylmethyl ester, (7S,10S,15S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: (S)-2-[((S)-3-Amino-butyrylamino)-methyl]-4-methyl-pentanoic acid benzyl ester; hydrochloride

: 210346-16-0
(S)-2-{[(tert-butoxycarbonyl)amino]methyl}-4-methylbutanoic acid

: 200400-98-2
(S)-2-({(S)-3-[(S)-2-(tert-Butoxycarbonylamino-methyl)-3-methyl-butyrylamino]-butyrylamino}-methyl)-4-methyl-pentanoic acid benzyl ester

Guidance literature:: With 4-methyl-morpholine; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In dichloromethane; 1h, 0 deg C; 18 h, r.t.;
DOI:10.1002/hlca.19980810513

Reference yield:

: 200400-96-0
(S)-2-[((S)-3-tert-Butoxycarbonylamino-butyrylamino)-methyl]-4-methyl-pentanoic acid benzyl ester

: 200400-98-2
(S)-2-({(S)-3-[(S)-2-(tert-Butoxycarbonylamino-methyl)-3-methyl-butyrylamino]-butyrylamino}-methyl)-4-methyl-pentanoic acid benzyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: HCl / dioxane / 2 h / 20 °C

2: 91 percent / 1-hydroxy-1H-benzotriazole, N-methylmorpholine, 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide / CH₂Cl₂ / 1h, 0 deg C; 18 h, r.t.

With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In 1,4-dioxane; dichloromethane;
DOI:10.1002/hlca.19980810513

Reference yield:

: H-(S)β²hLeu-OBn p-toluenesulfonate

: 200400-98-2
(S)-2-({(S)-3-[(S)-2-(tert-Butoxycarbonylamino-methyl)-3-methyl-butyrylamino]-butyrylamino}-methyl)-4-methyl-pentanoic acid benzyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 77 percent / 1-hydroxy-1H-benzotriazole, N-methylmorpholine, 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide / tetrahydrofuran / 1h, 0 deg C; 18 h, r.t.

2: HCl / dioxane / 2 h / 20 °C

3: 91 percent / 1-hydroxy-1H-benzotriazole, N-methylmorpholine, 1-<3-(dimethylamino)propyl>-3-ethylcarbodiimide / CH₂Cl₂ / 1h, 0 deg C; 18 h, r.t.

With 4-methyl-morpholine; hydrogenchloride; benzotriazol-1-ol; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In tetrahydrofuran; 1,4-dioxane; dichloromethane;
DOI:10.1002/hlca.19980810513