2,2'-Ethylenedioxydiphenol

Base Information

• Chemical Name: 2,2'-Ethylenedioxydiphenol
• CAS No.: 20115-81-5
• Molecular Formula: C14H14O4
• Molecular Weight: 246.263
• Hs Code.: 2909500000
• European Community (EC) Number: 680-023-6
• DSSTox Substance ID: DTXSID30409128
• Nikkaji Number: J1.070.025F
• Wikidata: Q82214831
• Mol file: 20115-81-5.mol

Synonyms:20115-81-5;2,2'-Ethylenedioxydiphenol;2,2'-(Ethane-1,2-diylbis(oxy))diphenol;2-[2-(2-hydroxyphenoxy)ethoxy]phenol;1,2-Bis(2-hydroxyphenoxy)ethane;Phenol, 2,2'-[1,2-ethanediylbis(oxy)]bis-;2,2-Ethylenedioxydiphenol;SCHEMBL2637278;1,2-bis(o-hydroxyphenoxy)ethane;DTXSID30409128;MFCD00441177;AKOS001579617;CCG-103645;3-BENZYL-4-METHYLTHIAZOLIUMCHLORIDE;Ethylene Glycol Bis(2-hydroxyphenyl) Ether;CS-0324042;E0557;T72037;A879828;SR-01000395321;SR-01000395321-1

Chemical Property of 2,2'-Ethylenedioxydiphenol

Chemical Property:

• Boiling Point: 434.8oC at 760 mmHg
• Flash Point: 216.8oC
• PSA: 58.92000
• Density: 1.261g/cm3
• LogP: 2.55560
• XLogP3: 2.8
• Hydrogen Bond Donor Count: 2
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 5
• Exact Mass: 246.08920892
• Heavy Atom Count: 18
• Complexity: 210

Purity/Quality:

97% ^*data from raw suppliers

2,2'-Ethylenedioxydiphenol >98.0%(GC) ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-36

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C(=C1)O)OCCOC2=CC=CC=C2O

Technology Process of 2,2'-Ethylenedioxydiphenol

There total 8 articles about 2,2'-Ethylenedioxydiphenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

2,2'-(Ethylendioxy)diphenoldibenzylether (73961-19-0) → 1,2-bis(o-hydroxyphenoxy)ethane (20115-81-5)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; at 25 ℃; for 4h; under 2280 Torr;

DOI:10.1021/jo00003a055

Reference yield: 80.0%

1,2-bis(2’-methoxyphenoxy)ethane (553-45-7) → 1,2-bis(o-hydroxyphenoxy)ethane (20115-81-5)

Guidance literature:

With 2,4,6-trimethyl-pyridine; lithium iodide; at 150 ℃; for 3h; Inert atmosphere;

DOI:10.3998/ark.5550190.0011.717

Reference yield: 77.0%

C24H30O6 → 1,2-bis(o-hydroxyphenoxy)ethane (20115-81-5)

Guidance literature:

With hydrogenchloride; In methanol; dichloromethane; water;

DOI:10.3998/ark.5550190.0011.717

upstream raw materials:

phenol 2-[(tetrahydro-2H-pyran-2yl)oxy]

ethylene dibromide

2,2'-(Ethylendioxy)diphenoldibenzylether

benzene-1,2-diol

Downstream raw materials:

2-<2-<2-(2-hydroxyphenoxy)ethoxy>phenoxy>ethanol

2-(2-{2-[2-(1-Carboxy-1-methyl-ethoxy)-phenoxy]-ethoxy}-phenoxy)-2-methyl-propionic acid

2,2'-(1,2-Ethandiyloxy)bisphenol-didodecylether

1,2-bis-<-(1-carboxydecyloxy)phenoxy>ethane