(R)-4-((3R,5R,8S,9S,10S,13R,14S,17R)-3-Acetoxy-10,13-dimethyl-11-oxo-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 10-phenylsulfanyl-9,10-dihydro-phenanthren-9-yl ester

Base Information

Chemical Name:(R)-4-((3R,5R,8S,9S,10S,13R,14S,17R)-3-Acetoxy-10,13-dimethyl-11-oxo-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 10-phenylsulfanyl-9,10-dihydro-phenanthren-9-yl ester
CAS No.:75927-88-7
Molecular Formula:C₄₆H₅₄O₅S
Molecular Weight:718.998
Hs Code.:

(R)-4-((3R,5R,8S,9S,10S,13R,14S,17R)-3-Acetoxy-10,13-dimethyl-11-oxo-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 10-phenylsulfanyl-9,10-dihydro-phenanthren-9-yl ester

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Chemical Property of (R)-4-((3R,5R,8S,9S,10S,13R,14S,17R)-3-Acetoxy-10,13-dimethyl-11-oxo-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 10-phenylsulfanyl-9,10-dihydro-phenanthren-9-yl ester

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Technology Process of (R)-4-((3R,5R,8S,9S,10S,13R,14S,17R)-3-Acetoxy-10,13-dimethyl-11-oxo-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 10-phenylsulfanyl-9,10-dihydro-phenanthren-9-yl ester

There total 3 articles about (R)-4-((3R,5R,8S,9S,10S,13R,14S,17R)-3-Acetoxy-10,13-dimethyl-11-oxo-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 10-phenylsulfanyl-9,10-dihydro-phenanthren-9-yl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 585-08-0,84489-06-5
phenanthrene-9,10-oxide

: 75927-88-7
(R)-4-((3R,5R,8S,9S,10S,13R,14S,17R)-3-Acetoxy-10,13-dimethyl-11-oxo-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 10-phenylsulfanyl-9,10-dihydro-phenanthren-9-yl ester

Guidance literature:: Multi-step reaction with 2 steps

2: dicyclohexylcarbodi-imide, 4-dimethylaminopyridine

With dmap; dicyclohexyl-carbodiimide;
DOI:10.1039/c39800000732

Reference yield:

: 13133-62-5
thiophenolate

: 75927-88-7
(R)-4-((3R,5R,8S,9S,10S,13R,14S,17R)-3-Acetoxy-10,13-dimethyl-11-oxo-hexadecahydro-cyclopenta[a]phenanthren-17-yl)-pentanoic acid 10-phenylsulfanyl-9,10-dihydro-phenanthren-9-yl ester

Guidance literature:: Multi-step reaction with 2 steps

2: dicyclohexylcarbodi-imide, 4-dimethylaminopyridine

With dmap; dicyclohexyl-carbodiimide;
DOI:10.1039/c39800000732