Technology Process of 2,9-Decadienoic acid,
5-[(4-methoxyphenyl)methoxy]-4,6-dimethyl-7-[(triethylsilyl)oxy]-, ethyl
ester, (2E,4S,5R,6R,7R)-
There total 9 articles about 2,9-Decadienoic acid,
5-[(4-methoxyphenyl)methoxy]-4,6-dimethyl-7-[(triethylsilyl)oxy]-, ethyl
ester, (2E,4S,5R,6R,7R)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 10 steps
1: TfOH / diethyl ether
2: TBAF / tetrahydrofuran
3: DMAP, pyridine
4: OsO4, NMO
5: NaIO4 / tetrahydrofuran; H2O
6: BF3*Et2O / -78 °C
7: 2,6-lutidine
8: DIBAL / hexane
9: Swern oxidation
10: NaHMDS
With
pyridine; 2,6-dimethylpyridine; dmap; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; trifluorormethanesulfonic acid; boron trifluoride diethyl etherate; tetrabutyl ammonium fluoride; sodium hexamethyldisilazane; diisobutylaluminium hydride;
In
tetrahydrofuran; diethyl ether; hexane; water;
DOI:10.1016/S0040-4039(97)10475-0
- Guidance literature:
-
Multi-step reaction with 8 steps
1: DMAP, pyridine
2: OsO4, NMO
3: NaIO4 / tetrahydrofuran; H2O
4: BF3*Et2O / -78 °C
5: 2,6-lutidine
6: DIBAL / hexane
7: Swern oxidation
8: NaHMDS
With
pyridine; 2,6-dimethylpyridine; dmap; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; boron trifluoride diethyl etherate; sodium hexamethyldisilazane; diisobutylaluminium hydride;
In
tetrahydrofuran; hexane; water;
DOI:10.1016/S0040-4039(97)10475-0
- Guidance literature:
-
Multi-step reaction with 7 steps
1: OsO4, NMO
2: NaIO4 / tetrahydrofuran; H2O
3: BF3*Et2O / -78 °C
4: 2,6-lutidine
5: DIBAL / hexane
6: Swern oxidation
7: NaHMDS
With
2,6-dimethylpyridine; sodium periodate; osmium(VIII) oxide; N-methyl-2-indolinone; boron trifluoride diethyl etherate; sodium hexamethyldisilazane; diisobutylaluminium hydride;
In
tetrahydrofuran; hexane; water;
DOI:10.1016/S0040-4039(97)10475-0