1-Piperidinecarboxylic acid, 4-[3-[(methylsulfonyl)oxy]propyl]-, 1,1-dimethylethyl ester

Base Information

• Chemical Name: 1-Piperidinecarboxylic acid, 4-[3-[(methylsulfonyl)oxy]propyl]-, 1,1-dimethylethyl ester
• CAS No.: 203859-94-3
• Molecular Formula: C14H27NO5S
• Molecular Weight: 321.438

Synonyms:tert-butyl 4-(3-((methylsulfonyl)oxy)propyl)piperidine-1-carboxylate;tert-butyl 4-{3-[(methylsulfonyl)oxy]propyl}piperidine-1-carboxylate;1-Boc-4-(2-((methylsulfonyl)oxy)propyl)piperidine;tert-butyl 4-[3-(methylsulfonyloxy)propyl]piperidinecarboxylate;4-(3-methanesulfonyloxypropyl)piperidine-1-carboxylic acid tert-butyl ester;4-(3-methanesulfonyloxy-propyl)-piperidine-1-carboxylic acid tert-butyl ester;

Chemical Property of 1-Piperidinecarboxylic acid, 4-[3-[(methylsulfonyl)oxy]propyl]-, 1,1-dimethylethyl ester

Chemical Property:

• PSA: 81.29000
• LogP: 3.40860

Purity/Quality:

99% ^*data from raw suppliers

3-(1-Tert-butoxycarbonyl-4-piperidyl)-1-propylmesylate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Piperidinecarboxylic acid, 4-[3-[(methylsulfonyl)oxy]propyl]-, 1,1-dimethylethyl ester

There total 4 articles about 1-Piperidinecarboxylic acid, 4-[3-[(methylsulfonyl)oxy]propyl]-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

methanesulfonyl chloride (124-63-0) + N-Boc-piperidin-4-yl-propanol (156185-63-6) → 4-(3-Methanesulfonyloxy-propyl)-piperidine-1-carboxylic acid tert-butyl ester (203859-94-3)

Guidance literature:

With triethylamine; In dichloromethane; at 0 ℃; for 1h;

Reference yield:

2-(Dimethylamino)pyridine (5683-33-0) + 4-(3-Hydroxypropyl)pyridine (2629-72-3) + methanesulfonyl chloride (124-63-0) + N-Boc-piperidin-4-yl-propanol (156185-63-6) → 4-(3-Methanesulfonyloxy-propyl)-piperidine-1-carboxylic acid tert-butyl ester (203859-94-3)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In tetrahydrofuran;

Reference yield:

N-(3-bromo-4-(1H-imidazol-1-yl)phenyl)-5-(3,5-dimethylisoxazol-4-yl)-2-methylaniline → 4-(3-Methanesulfonyloxy-propyl)-piperidine-1-carboxylic acid tert-butyl ester (203859-94-3)

Guidance literature:

upstream raw materials:

methanesulfonyl chloride

N-Boc-piperidin-4-yl-propanol

2-(Dimethylamino)pyridine

4-(3-Hydroxypropyl)pyridine

Downstream raw materials:

4-[3-(4-bromo-3,5-dimethylphenoxy)propyl]piperidine-1-carboxylic acid tert-butyl ester

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