{(1,3-diphenylpropane-1,3-dionato)bis(ethylenediamine)cobalt(III) perchlorate}*HClO₄

Base Information

• Chemical Name: {(1,3-diphenylpropane-1,3-dionato)bis(ethylenediamine)cobalt(III) perchlorate}*HClO₄
• CAS No.: 113774-77-9
• Molecular Formula: C₁₉H₂₇CoN₄O₂*ClHO₄*2ClO₄
• Molecular Weight: 701.802

Synonyms:

Chemical Property of {(1,3-diphenylpropane-1,3-dionato)bis(ethylenediamine)cobalt(III) perchlorate}*HClO₄

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of {(1,3-diphenylpropane-1,3-dionato)bis(ethylenediamine)cobalt(III) perchlorate}*HClO₄

There total 1 articles about {(1,3-diphenylpropane-1,3-dionato)bis(ethylenediamine)cobalt(III) perchlorate}*HClO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cis-{cobalt(ethylenediamine)2(N3)2} perchlorate (14877-87-3) + triethyl phosphate (78-40-0) + sodium perchlorate + nitrosonium tetrafluoroborate + 1,3-diphenylpropanedione (120-46-7,61346-73-4) → {(1,3-diphenylpropane-1,3-dionato)bis(ethylenediamine)cobalt(III) perchlorate}*HClO4 (113774-77-9)

Guidance literature:

In further solvent(s); Addn. of NOBF4 to dried triethyl phosphate, {Co(en)2(N3)2}(ClO4) is added in several portions, when evolution of gases ceases dibenzoylmethane is added. The soln. is heated on a steam bath for 60 h with occasional swirling.; The cooled react. mixt. is poured into stirred Et2O, the resulting solid is ion-exchanged (CM-Sephadex C-25-120, aq. NaCl), column chromy. (orange band), addn. of solid NaClO4 yields orange ppt., elem. anal.;

Reference yield:

{(1,3-diphenylpropane-1,3-dionato)bis(ethylenediamine)cobalt(III) perchlorate}*HClO4 (113774-77-9) + chromium (II) (22541-79-3) → {Cr(II)(OH2)5(1,3-diphenylpropane-1,3-dionato)}(1+) (113705-88-7)

Guidance literature:

React. between {Co(en)2(dppd)}(2+) and Cr(II).; Rapid ion-exchange on SP-Sephadex (SP-25-120, aq. NaCl).;

upstream raw materials:

cis-{cobalt(ethylenediamine)2(N₃)2} perchlorate

triethyl phosphate

1,3-diphenylpropanedione

Downstream raw materials:

{Cr(II)(OH₂)5(1,3-diphenylpropane-1,3-dionato)}⁽¹⁺⁾

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