1-(2-Chloroethyl)-3-nitrobenzene

Base Information

Chemical Name:1-(2-Chloroethyl)-3-nitrobenzene
CAS No.:20849-75-6
Molecular Formula:C8H8ClNO2
Molecular Weight:185.61
Hs Code.:
DSSTox Substance ID:DTXSID20494321
Wikidata:Q82341595
Mol file:20849-75-6.mol

Synonyms:1-(2-Chloroethyl)-3-nitrobenzene;20849-75-6;1-CHLORO-2-(3-NITROPHENYL)ETHANE;SCHEMBL365344;DTXSID20494321;AKOS006323282

Suppliers and Price of 1-(2-Chloroethyl)-3-nitrobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1-(2-Chloroethyl)-3-nitrobenzene

Chemical Property:

Boiling Point:304.4±17.0 °C(Predicted)
PSA：45.82000
Density:1.275±0.06 g/cm3(Predicted)
LogP:2.89930
XLogP3:2.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:185.0243562
Heavy Atom Count:12
Complexity:158

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC(=C1)[N+](=O)[O-])CCCl

Technology Process of 1-(2-Chloroethyl)-3-nitrobenzene

There total 4 articles about 1-(2-Chloroethyl)-3-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 52022-77-2
2-(3-nitrophenyl)ethanol

: 20849-75-6
1-(2-chloroethyl)-3-nitrobenzene

Guidance literature:: With dmap; triethylamine; p-toluenesulfonyl chloride; In dichloromethane; at 20 ℃; for 3h;

Reference yield:

: 74-85-1
ethene

: 2865-17-0
m-nitrophenylmercury(II) chloride

: 20849-75-6
1-(2-chloroethyl)-3-nitrobenzene

Guidance literature:: With lithium chloride; copper dichloride; lithium tetrachloropalladate(II); In acetic acid;
DOI:10.1021/ja01022a038

Reference yield:

: 10268-12-9
methyl 3-nitrophenylacetate

: 20849-75-6
1-(2-chloroethyl)-3-nitrobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: methanol; sodium tetrahydroborate / tetrahydrofuran / 0 - 20 °C

2: thionyl chloride / 3 h / 70 °C

With methanol; sodium tetrahydroborate; thionyl chloride; In tetrahydrofuran;