ethyl alpha-[[4-[bis(2-chloroethyl)amino]phenyl]methyl]-1,3-dihydro-1,3-dioxo-2H-isoindole-2-acetate

Base Information

• Chemical Name: ethyl alpha-[[4-[bis(2-chloroethyl)amino]phenyl]methyl]-1,3-dihydro-1,3-dioxo-2H-isoindole-2-acetate
• CAS No.: 93942-39-3
• Molecular Formula: C₂₃H₂₄Cl₂N₂O₄
• Molecular Weight: 463.361
• Mol file: 93942-39-3.mol

Synonyms:ethyl alpha-[[4-[bis(2-chloroethyl)amino]phenyl]methyl]-1,3-dihydro-1,3-dioxo-2H-isoindole-2-acetate

Chemical Property of ethyl alpha-[[4-[bis(2-chloroethyl)amino]phenyl]methyl]-1,3-dihydro-1,3-dioxo-2H-isoindole-2-acetate

Chemical Property:

• Boiling Point: 612°Cat760mmHg
• Flash Point: 324°C
• PSA: 66.92000
• Density: 1.34g/cm³
• LogP: 3.67890

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ethyl alpha-[[4-[bis(2-chloroethyl)amino]phenyl]methyl]-1,3-dihydro-1,3-dioxo-2H-isoindole-2-acetate

There total 18 articles about ethyl alpha-[[4-[bis(2-chloroethyl)amino]phenyl]methyl]-1,3-dihydro-1,3-dioxo-2H-isoindole-2-acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

N-phthalimido-4-(bis-2-ethylsulfate)amino-L-phenylalanine ethyl ester → N-phthalimido-4-(bis-2-chloroethyl)amino-L-phenylalanine ethyl ester (792864-20-1,93942-39-3)

Guidance literature:

With calcium chloride; In acetonitrile; at 60 ℃; for 13h; Solvent; Reagent/catalyst; Temperature;

Reference yield: 97.1%

C23H26N2O6 → C23H24Cl2N2O4 (93942-39-3)

Guidance literature:

With trichlorophosphate; In toluene; at 0 - 70 ℃; for 0.16h;

Reference yield: 95.3%

N-phthalimido-4-(bis-2-hydroxyethyl)amino-L-phenylalanine ethyl ester (97338-02-8) → N-phthalimido-4-(bis-2-chloroethyl)amino-L-phenylalanine ethyl ester (792864-20-1,93942-39-3)

Guidance literature:

With trichlorophosphate; In toluene; at 10 - 70 ℃; for 0.16h; Temperature;

upstream raw materials:

N-phthalimido-4-(bis-2-hydroxyethyl)amino-L-phenylalanine ethyl ester

N-phthalimido-4-nitro-L-phenylalanine ethyl ester

1-chloro-2-iodoethane

N-phthalimido-4-amino-L-phenylalanine ethyl ester

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