1,2-Butanediol, 4-(4-methoxyphenoxy)-2-methyl-, (2S)-

Base Information

Chemical Name:1,2-Butanediol, 4-(4-methoxyphenoxy)-2-methyl-, (2S)-
CAS No.:209118-78-5
Molecular Formula:C12H18O4
Molecular Weight:226.273
Hs Code.:
DSSTox Substance ID:DTXSID10454318
Nikkaji Number:J975.038J
Wikidata:Q82275775

Synonyms:209118-78-5;(S)-4-(4-Methoxyphenoxy)-2-methylbutane-1,2-diol;1,2-Butanediol, 4-(4-methoxyphenoxy)-2-methyl-, (2S)-;starbld0028295;SCHEMBL23539109;DTXSID10454318;(S)-2-Methyl-4-(4-methoxyphenoxy)-1,2-butanediol

Suppliers and Price of 1,2-Butanediol, 4-(4-methoxyphenoxy)-2-methyl-, (2S)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 1,2-Butanediol, 4-(4-methoxyphenoxy)-2-methyl-, (2S)-

Chemical Property:

XLogP3:1.1
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:226.12050905
Heavy Atom Count:16
Complexity:190

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(CCOC1=CC=C(C=C1)OC)(CO)O
Isomeric SMILES:C[C@](CCOC1=CC=C(C=C1)OC)(CO)O

Technology Process of 1,2-Butanediol, 4-(4-methoxyphenoxy)-2-methyl-, (2S)-

There total 6 articles about 1,2-Butanediol, 4-(4-methoxyphenoxy)-2-methyl-, (2S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 169310-73-0
1-methoxy-4-((3-methylbut-3-en-1-yl)oxy)benzene

: 209118-78-5
(2S)-4-(4-methoxyphenoxy)-2-methylbutane-1,2-diol

Guidance literature:: With asymmetric dihydroxylation-mix-α; hydroquinidein 1,4-phthalazinediyl diether; In water; tert-butyl alcohol; at 0 ℃; for 24h; Inert atmosphere;
DOI:10.1021/ol203064r

Reference yield:

: 150-76-5
4-methoxy-phenol

: 209118-78-5
(2S)-4-(4-methoxyphenoxy)-2-methylbutane-1,2-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / EtO₂CN=NCO₂Et; Ph₃P / tetrahydrofuran / 4 h / Heating

2: 98 percent / AD-mix-α / H2O; 2-methyl-propan-2-ol / 2 h / 0 °C

With AD-mix-α; triphenylphosphine; diethylazodicarboxylate; In tetrahydrofuran; water; tert-butyl alcohol;
DOI:10.1055/s-2006-932487

Reference yield:

: 763-32-6
2-methyl-1-buten-4-ol

: 209118-78-5
(2S)-4-(4-methoxyphenoxy)-2-methylbutane-1,2-diol

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / PPh₃, diisopropyl azodicarboxylate / CH₂Cl₂ / 3 h / Ambient temperature

2: 93 percent / AD-mix-α<(DHQ)2PHAL>, H2O / 2-methyl-propan-2-ol / 24 h / 4 °C

With AD-mix-α; di-isopropyl azodicarboxylate; water; triphenylphosphine; In dichloromethane; tert-butyl alcohol;
DOI:10.1055/s-1998-2076