Phenyl(prop-2-en-1-yl)cyanamide

Base Information

Chemical Name:Phenyl(prop-2-en-1-yl)cyanamide
CAS No.:20914-24-3
Molecular Formula:C10H10N2
Molecular Weight:158.203
Hs Code.:
DSSTox Substance ID:DTXSID60573447
Nikkaji Number:J1.376.165E
Wikidata:Q82462175

Synonyms:Phenyl(prop-2-en-1-yl)cyanamide;20914-24-3;SCHEMBL2582845;DTXSID60573447;InChI=1/C10H10N2/c1-2-8-12(9-11)10-6-4-3-5-7-10/h2-7H,1,8H

Suppliers and Price of Phenyl(prop-2-en-1-yl)cyanamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of Phenyl(prop-2-en-1-yl)cyanamide

Chemical Property:

XLogP3:2.7
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:158.084398327
Heavy Atom Count:12
Complexity:183

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=CCN(C#N)C1=CC=CC=C1

Technology Process of Phenyl(prop-2-en-1-yl)cyanamide

There total 6 articles about Phenyl(prop-2-en-1-yl)cyanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 55305-43-6
N-cyano-N-phenyl-p-toluenesulfonamide

: 107-18-6
allyl alcohol

: 20914-24-3
N-allyl-N-phenylcyanamide

Guidance literature:: allyl alcohol; With tetra-(n-butyl)ammonium iodide; sodium tert-pentoxide; In tetrahydrofuran; at 25 ℃; Sealed tube; Inert atmosphere;

N-cyano-N-phenyl-p-toluenesulfonamide; In tetrahydrofuran; at 25 ℃; for 16h; Sealed tube; Inert atmosphere;
DOI:10.1021/acs.orglett.7b01710

Reference yield:

: 589-09-3
N-allyl-N-phenylamine

: 506-68-3
bromocyane

: 20914-24-3
N-allyl-N-phenylcyanamide

Guidance literature:: at 50 ℃;

Reference yield:

: 64-10-8
phenyl carbamate

: 20914-24-3
N-allyl-N-phenylcyanamide

Guidance literature:: Multi-step reaction with 2 steps

1.1: pyridine / 0.25 h / 25 °C / Sealed tube; Inert atmosphere

2.1: sodium tert-pentoxide; tetra-(n-butyl)ammonium iodide / tetrahydrofuran / 25 °C / Sealed tube; Inert atmosphere

2.2: 16 h / 25 °C / Sealed tube; Inert atmosphere

With pyridine; tetra-(n-butyl)ammonium iodide; sodium tert-pentoxide; In tetrahydrofuran;
DOI:10.1021/acs.orglett.7b01710