1H-Pyrido[3,4-b]indole-3-carboxylic acid, 2,3,4,9-tetrahydro-1-phenyl-, (3S)-

Base Information

• Chemical Name: 1H-Pyrido[3,4-b]indole-3-carboxylic acid, 2,3,4,9-tetrahydro-1-phenyl-, (3S)-
• CAS No.: 209169-30-2
• Molecular Formula: C18H16N2O2
• Molecular Weight: 292.337

Synonyms:1-phenyl-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid;(3S)-1-phenyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid;1-phenyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid;1-Phenyl-2,3,4,9-tetrahydro-1H-β-carbolin-3-carbonsaeure;

Chemical Property of 1H-Pyrido[3,4-b]indole-3-carboxylic acid, 2,3,4,9-tetrahydro-1-phenyl-, (3S)-

Chemical Property:

• PSA: 65.12000
• LogP: 3.18500

Purity/Quality:

(3S)-1-phenyl-2,3,4,9-tetrahydro-1H-pyrido[3,4-b]indole-3-carboxylicacid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1H-Pyrido[3,4-b]indole-3-carboxylic acid, 2,3,4,9-tetrahydro-1-phenyl-, (3S)-

There total 4 articles about 1H-Pyrido[3,4-b]indole-3-carboxylic acid, 2,3,4,9-tetrahydro-1-phenyl-, (3S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

benzaldehyde (100-52-7) + L-Tryptophan (73-22-3,27732-43-0,80206-30-0,27813-82-7) → (3S)-1-phenyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid (209169-30-2)

Guidance literature:

With acetic acid; for 2h; Reflux;

DOI:10.1016/j.bmc.2014.08.035

Reference yield: 89.0%

→ (3S)-1-phenyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid (209169-30-2)

Guidance literature:

With acetic acid; for 3h; Reflux;

Reference yield:

Boc-Trp-OH (13139-14-5) + benzaldehyde (100-52-7) → (3S)-1-phenyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid (209169-30-2)

Guidance literature:

Yield given; Multistep reaction;

DOI:10.1002/(SICI)1521-3773(19980504)37:8<1143::AID-ANIE1143>3.0.CO;2-E

upstream raw materials:

benzaldehyde

L-Tryptophan

Boc-Trp-OH

Downstream raw materials:

(3S)-1-phenyl-1,2,3,4-tetrahydro-β-carboline-3-carboxylic acid methyl ester

1-phenyl-9H-pyrido[3,4-b]indole

1-phenyl-9-(3-phenylpropyl)-β-carboline

9-(3-phenylpropyl)-2-benzyl-1-phenyl-β-carbolinium bromide

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