Phenol, 2-[[[2,6-bis(1-methylethyl)phenyl]imino]methyl]-4,6-dichloro-

Base Information

Chemical Name:Phenol, 2-[[[2,6-bis(1-methylethyl)phenyl]imino]methyl]-4,6-dichloro-
CAS No.:210882-40-9
Molecular Formula:C₁₉H₂₁Cl₂NO
Molecular Weight:350.288
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenol, 2-[[[2,6-bis(1-methylethyl)phenyl]imino]methyl]-4,6-dichloro-

Chemical Property:

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Technology Process of Phenol, 2-[[[2,6-bis(1-methylethyl)phenyl]imino]methyl]-4,6-dichloro-

There total 1 articles about Phenol, 2-[[[2,6-bis(1-methylethyl)phenyl]imino]methyl]-4,6-dichloro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24544-04-5
2,6-diisopropylbenzenamine

: 90-60-8
3,5-dichlorosalicyclaldehyde

: 210882-40-9
4,6-dichloro-2-[[(2,6-diisopropylphenyl)imino]methyl]phenol

Guidance literature:: In methanol; for 0.5h;
DOI:10.1002/ejic.200801049

Reference yield: 96.8%

: (N,N,N',N'-tetramethylethylenediamine)dimethylpalladium(II)

: 210882-40-9
4,6-dichloro-2-[[(2,6-diisopropylphenyl)imino]methyl]phenol

: 63249-99-0
3,5-diacetyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonanee

: 685867-70-3
[Pd(CH₃)((2,4-Cl₂C₆H₂OCHNC₆H₃-2,6-i-Pr)(3,7-diacetyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane)]

Guidance literature:: In methanol; toluene; byproducts: CH4, TMEDA; to a soln. of Pd-complex in toluene at -30°C was added phosphine in methanol, then salicylaldimine in toluene was added at -30°C, the soln. was stirred for 30 min, allowed to warm to room temp., stirredovernight (inert atm.); the solvent was removed in vac., cold pentane was added, ppt. was filtered, washed with cold (-78°C) pentane; elem. anal.;
DOI:10.1021/om0343059

Reference yield: 94.0%

: bis(bis(trimethylsilyl)amido)zinc(II)

: 210882-40-9
4,6-dichloro-2-[[(2,6-diisopropylphenyl)imino]methyl]phenol

: 331624-19-2
Zn(Cl₂C₆H₂OCHNC₆H₃(C₃H₇)2)2

Guidance literature:: In pentane; ligand was dissolved in pentane, soln. of Zn-complex in pentane was added; filtered, washed with pentane; elem. anal.;
DOI:10.1021/ic0006403