3,7-Diacetyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane

Base Information

Chemical Name:3,7-Diacetyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane
CAS No.:63249-99-0
Molecular Formula:C9H16N3O2P
Molecular Weight:229.219
Hs Code.:
DSSTox Substance ID:DTXSID40478880
Nikkaji Number:J2.029.126E
Wikidata:Q82312579

Synonyms:3,7-diacetyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane;63249-99-0;1-(7-acetyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonan-3-yl)ethanone;SCHEMBL4210915;DTXSID40478880;1,3,7-Triaza-5-phosphabicyclo[3.3.1]nonane, 3,7-diacetyl-;3,7-Diacetyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane, 97%

Suppliers and Price of 3,7-Diacetyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3,7-Diacetyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane

Chemical Property:

XLogP3:-1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:229.09801376
Heavy Atom Count:15
Complexity:271

Purity/Quality:: 98%,99%, ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=O)N1CN2CN(CP(C2)C1)C(=O)C

Technology Process of 3,7-Diacetyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane

There total 1 articles about 3,7-Diacetyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: 53597-69-6
(1,3,5-triaza-7-phosphaadamantane)

: 63249-99-0
3,5-diacetyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonanee

Guidance literature:

Reference yield: 96.8%

: (N,N,N',N'-tetramethylethylenediamine)dimethylpalladium(II)

: 210882-40-9
4,6-dichloro-2-[[(2,6-diisopropylphenyl)imino]methyl]phenol

: 63249-99-0
3,5-diacetyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonanee

: 685867-70-3
[Pd(CH₃)((2,4-Cl₂C₆H₂OCHNC₆H₃-2,6-i-Pr)(3,7-diacetyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane)]

Guidance literature:: In methanol; toluene; byproducts: CH4, TMEDA; to a soln. of Pd-complex in toluene at -30°C was added phosphine in methanol, then salicylaldimine in toluene was added at -30°C, the soln. was stirred for 30 min, allowed to warm to room temp., stirredovernight (inert atm.); the solvent was removed in vac., cold pentane was added, ppt. was filtered, washed with cold (-78°C) pentane; elem. anal.;
DOI:10.1021/om0343059

Reference yield: 93.0%

: palladium dichloride

: 63249-99-0
3,5-diacetyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonanee

: cis-[bis(3,7-diacetyl-1,3,7-triaza-5-phosphabicyclo[3.3.1]nonane)dichloridopalladium(II)]

Guidance literature:: In dichloromethane; suspn. of PdCl2 in CH2Cl2 treated with ligand (Pd:L=1:2), stirred for 24h; filtered, washed (CH2Cl2), dried (vac.), elem. anal.;
DOI:10.1002/ejic.200700112