Gly-L-Asu-L-PheOH

Base Information

• Chemical Name: Gly-L-Asu-L-PheOH
• CAS No.: 623901-65-5
• Molecular Formula: C₁₅H₁₇N₃O₅
• Molecular Weight: 319.317

Synonyms:

Chemical Property of Gly-L-Asu-L-PheOH

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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Technology Process of Gly-L-Asu-L-PheOH

There total 4 articles about Gly-L-Asu-L-PheOH which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

H-Gly-Asp-Phe-OH → Gly-L-Asu-L-PheOH (623901-65-5)

Guidance literature:

With hydrogenchloride; acetic acid;

DOI:10.1002/jps.22134

Reference yield:

N-Fmoc L-Phe (35661-40-6) → Gly-L-Asu-L-PheOH (623901-65-5)

Guidance literature:

Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / solid phase reaction

1.2: solid phase reaction

2.1: hydrogenchloride; acetic acid

With hydrogenchloride; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; acetic acid;

DOI:10.1002/jps.22134

Reference yield:

N-Fmoc L-Phe (35661-40-6) → Gly-D-Asu-L-PheOH + Gly-L-Asu-L-PheOH (623901-65-5) + Gly-β-D-Asp-L-PheOH (455258-18-1) + Gly-β-L-Asp-L-PheOH (623901-63-3) + Gly-α-D-Asp-L-PheOH (924902-07-8)

Guidance literature:

Multi-step reaction with 2 steps

1.1: benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate / solid phase reaction

1.2: solid phase reaction

2.1: 80 °C / pH 10 / aq. buffer

With benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate;

DOI:10.1002/jps.22134

upstream raw materials:

N-Fmoc L-Phe

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