Technology Process of Benzene, 1,1',1''-(1-chloro-1,2-propadien-1-yl-3-ylidene)tris-
There total 3 articles about Benzene, 1,1',1''-(1-chloro-1,2-propadien-1-yl-3-ylidene)tris- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
methanesulfonyl chloride; triethylamine;
In
dichloromethane;
at 0 ℃;
for 1h;
Inert atmosphere;
DOI:10.1002/ejoc.201100033
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium phosphate; palladium diacetate; triethylamine; triphenylphosphine / acetonitrile / 0.5 h / Inert atmosphere
1.2: 12 h / 20 °C / Inert atmosphere
2.1: methanesulfonyl chloride; triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere
With
potassium phosphate; palladium diacetate; methanesulfonyl chloride; triethylamine; triphenylphosphine;
In
dichloromethane; acetonitrile;
1.1: Sonogashira coupling / 1.2: Sonogashira coupling;
DOI:10.1002/ejoc.201100033
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: potassium phosphate; palladium diacetate; triethylamine; triphenylphosphine / acetonitrile / 0.5 h / Inert atmosphere
1.2: 12 h / 20 °C / Inert atmosphere
2.1: methanesulfonyl chloride; triethylamine / dichloromethane / 1 h / 0 °C / Inert atmosphere
With
potassium phosphate; palladium diacetate; methanesulfonyl chloride; triethylamine; triphenylphosphine;
In
dichloromethane; acetonitrile;
1.1: Sonogashira coupling / 1.2: Sonogashira coupling;
DOI:10.1002/ejoc.201100033
