Benzenamine, 2,4-dichloro-N-sulfinyl-

Base Information

• Chemical Name: Benzenamine, 2,4-dichloro-N-sulfinyl-
• CAS No.: 21250-19-1
• Molecular Formula: C6H3Cl2NOS
• Molecular Weight: 208.068
• Mol file: 21250-19-1.mol

Synonyms:2,4-Dichlor-N-sulfinylanilin;2,4-Dichlor-N-sulfinyl-anilin;2,4-dichloro-N-sulfinyl-aniline;

Chemical Property of Benzenamine, 2,4-dichloro-N-sulfinyl-

Chemical Property:

• Melting Point: 66 - 68 °C
• PSA: 61.52000
• LogP: 3.88720

Purity/Quality:

99% ^*data from raw suppliers

2,4-Dichloro-1-(sulfinylamino)benzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of Benzenamine, 2,4-dichloro-N-sulfinyl-

There total 2 articles about Benzenamine, 2,4-dichloro-N-sulfinyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2,4-Dichloroaniline (554-00-7,51908-09-9) → N-(2,4-dichloro-phenyl)-sulfur imide oxide (21250-19-1)

Guidance literature:

With thionyl chloride;

DOI:10.1016/S0040-4039(00)01011-X

Reference yield:

→ N-(2,4-dichloro-phenyl)-sulfur imide oxide (21250-19-1)

Guidance literature:

2,4-Dichlor-anilin, Bzl., SOCl2;

Reference yield: 92.0%

N-(2,4-dichloro-phenyl)-sulfur imide oxide (21250-19-1) + vinyl magnesium bromide (1826-67-1) → N-(2,4-dichlorophenyl)ethenesulfinamide

Guidance literature:

In tetrahydrofuran; for 2h; -78 deg C to room temp.;

upstream raw materials:

2,4-Dichloroaniline

Downstream raw materials:

1-(2,4-dichloro-phenylimino)-7-nitro-5-trifluoromethyl-1H-1λ⁴-benzothiazole-2-carboxylic acid ethyl ester

1-(2,4-dichloro-phenylimino)-5,7-dinitro-1H-1λ⁴-benzothiazole-2-carboxylic acid ethyl ester

2-(2,4-dichloro-phenyl)-1-oxo-4,4-diphenyl-1λ⁴-[1,2]thiazetidin-3-one

2'-(2,4-dichloro-phenyl)-1'-oxo-1'λ⁴-spiro[fluorene-9,4'-[1,2]thiazetidin]-3'-one

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