BOC-GLU(OAL)-OAL

Base Information

• Chemical Name: BOC-GLU(OAL)-OAL
• CAS No.: 212569-21-6
• Molecular Formula: C16H25NO6
• Molecular Weight: 327.37300
• Mol file: 212569-21-6.mol

Synonyms:

Chemical Property of BOC-GLU(OAL)-OAL

Chemical Property:

• Boiling Point: 420.9±45.0 °C(Predicted)
• PKA: 10.96±0.46(Predicted)
• PSA: 90.93000
• Density: 1.082±0.06 g/cm3(Predicted)
• LogP: 2.50920

Purity/Quality:

99% ^*data from raw suppliers

(S)-Diallyl2-((tert-butoxycarbonyl)amino)pentanedioate 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of BOC-GLU(OAL)-OAL

There total 1 articles about BOC-GLU(OAL)-OAL which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

Boc-Glu (2419-94-5) + allyl alcohol (107-18-6) → C16H25NO6 (212569-21-6)

Guidance literature:

With 1-hydroxy-7-aza-benzotriazole; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 24h;

DOI:10.1016/j.tetlet.2009.03.130

Reference yield: 86.0%

C16H25NO6 (212569-21-6) → N-α-(t-butoxycarbonyl)-L-glutamic γ-allyl ester (132286-79-4,259221-91-5)

Guidance literature:

With Alcalase-cross-linked-enzyme-aggregates; In tert-butyl alcohol; at 37 ℃; for 16h; pH=7.5; regioselective reaction; aq. phosphate buffer; Enzymatic reaction;

DOI:10.1016/j.tetlet.2009.03.130

upstream raw materials:

Boc-Glu

allyl alcohol

Downstream raw materials:

N-α-(t-butoxycarbonyl)-L-glutamic γ-allyl ester