Phosphine sulfide, diphenyl[(1Z)-2-phenylethenyl]-

Base Information

Chemical Name:Phosphine sulfide, diphenyl[(1Z)-2-phenylethenyl]-
CAS No.:21298-89-5
Molecular Formula:C20H17PS
Molecular Weight:320.395
Hs Code.:

Synonyms:

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Chemical Property of Phosphine sulfide, diphenyl[(1Z)-2-phenylethenyl]-

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Technology Process of Phosphine sulfide, diphenyl[(1Z)-2-phenylethenyl]-

There total 10 articles about Phosphine sulfide, diphenyl[(1Z)-2-phenylethenyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

: 536-74-3
phenylacetylene

: 829-85-6
diphenylphosphane

: 21298-89-5
diphenyl[(Z)-2-phenylethenyl]phosphine sulfide

Guidance literature:: With sulfur; In neat (no solvent); at 70 ℃; regioselective reaction; Green chemistry;
DOI:10.1039/c6gc00903d

Reference yield: 94.0%

: 6591-07-7
diphenylphosphane sulfide

: 536-74-3
phenylacetylene

: 21298-89-5
diphenyl[(Z)-2-phenylethenyl]phosphine sulfide

Guidance literature:: In neat (no solvent); at 80 ℃; for 5h; stereoselective reaction; Inert atmosphere;
DOI:10.1002/ejoc.201301786

Reference yield:

: 829-85-6
diphenylphosphane

: 21298-89-5
diphenyl[(Z)-2-phenylethenyl]phosphine sulfide

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / S₈ / toluene / 2.5 h / 80 °C

2: 65 percent / AIBN / 70 °C

With sulfur; 2,2'-azobis(isobutyronitrile); In toluene;
DOI:10.1021/jo9622441