1-Methoxydibenzopentacyclo<7.2.2.0^2,7.0^2,8.0^3,8>trideca-10,12-dien

Base Information

• Chemical Name: 1-Methoxydibenzopentacyclo<7.2.2.0^2,7.0^2,8.0^3,8>trideca-10,12-dien
• CAS No.: 78379-94-9
• Molecular Formula: C₂₂H₂₀O
• Molecular Weight: 300.4

Synonyms:

Chemical Property of 1-Methoxydibenzopentacyclo<7.2.2.0^2,7.0^2,8.0^3,8>trideca-10,12-dien

Chemical Property:

Purity/Quality:

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Technology Process of 1-Methoxydibenzopentacyclo<7.2.2.0^2,7.0^2,8.0^3,8>trideca-10,12-dien

There total 4 articles about 1-Methoxydibenzopentacyclo<7.2.2.0^2,7.0^2,8.0^3,8>trideca-10,12-dien which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,3-diphenylisobenzofuran (5471-63-6) + 9-methoxyanthracene (2395-96-2,34516-97-7,84367-94-2) + 1-bromo-tricyclo<4.1.0.02,7>heptane (63846-85-5) → 1-Methoxydibenzopentacyclo<7.2.2.02,7.02,8.03,8>trideca-10,12-dien (78379-94-9) + 1,9-Diphenyl-12-oxabenzopentacyclo<7.2.1.02,7.02,8.03,8>dodec-10-en (71794-78-0)

Guidance literature:

With lithium diisopropyl amide; In tetrahydrofuran; at -20 ℃; Kinetics; Mechanism; relative rate constant, competition constant;

Reference yield:

1,3-diphenylisobenzofuran (5471-63-6) + 9-methoxyanthracene (2395-96-2,34516-97-7,84367-94-2) + 1-iodotricyclo<4.1.0.02,7>heptane (65131-65-9) → 1-Methoxydibenzopentacyclo<7.2.2.02,7.02,8.03,8>trideca-10,12-dien (78379-94-9) + 1,9-Diphenyl-12-oxabenzopentacyclo<7.2.1.02,7.02,8.03,8>dodec-10-en (71794-78-0)

Guidance literature:

With lithium diisopropyl amide; In tetrahydrofuran; at -20 ℃; Kinetics; Mechanism; relative rate constant, competition constant;

Reference yield:

1,3-diphenylisobenzofuran (5471-63-6) + 9-methoxyanthracene (2395-96-2,34516-97-7,84367-94-2) + tricyclo<4.1.0.02,7>hept-1(7)-ene (78365-77-2) → 1-Methoxydibenzopentacyclo<7.2.2.02,7.02,8.03,8>trideca-10,12-dien (78379-94-9) + 1,9-Diphenyl-12-oxabenzopentacyclo<7.2.1.02,7.02,8.03,8>dodec-10-en (71794-78-0)

Guidance literature:

With lithium diisopropyl amide; In tetrahydrofuran; at -20 ℃; for 1h; Kinetics; competition constant , further reagent: KOtBu;

upstream raw materials:

1,3-diphenylisobenzofuran

9-methoxyanthracene

1-Chlorotricyclo<4.1.0.0^2,7>heptane

1-bromo-tricyclo<4.1.0.0^2,7>heptane

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