(μEtSe)(μ-PhC=NPh)Fe2(CO)6

Base Information

Chemical Name:(μEtSe)(μ-PhC=NPh)Fe2(CO)6
CAS No.:353760-12-0
Molecular Formula:C₂₁H₁₅Fe₂NO₆Se
Molecular Weight:568.007
Hs Code.:

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Chemical Property of (μEtSe)(μ-PhC=NPh)Fe2(CO)6

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Technology Process of (μEtSe)(μ-PhC=NPh)Fe2(CO)6

There total 1 articles about (μEtSe)(μ-PhC=NPh)Fe2(CO)6 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 7782-49-2
selenium

: 17685-52-8
triiron dodecarbonyl

: 925-90-6
ethylmagnesium bromide

: 4903-36-0
N-phenyl-benzimidoyl chloride

: 38497-98-2
(μ-EtSe)2Fe2(CO)6

: 353760-12-0
(μEtSe)(μ-PhC=NPh)Fe2(CO)6

Guidance literature:: In tetrahydrofuran; diethyl ether; under N2 atm. to suspn. Se in THF was added EtMgBr in Et2O and stirred until Se was disappeared, Fe3(CO)12 was added and stirred for 0.5 h, mixt. was cooled to -78°C, PhC(Cl)=NPh in THF was added; mixt. was filtered, concd. under reduced pressure, chromy. (TLC, CH2Cl2-petroleum ether 1:20); elem. anal.;
DOI:10.1016/S0022-328X(01)00766-5