3-Cyclohexylideneoxolan-2-one

Base Information

Chemical Name:3-Cyclohexylideneoxolan-2-one
CAS No.:21681-63-0
Molecular Formula:C₁₀H₁₄O₂
Molecular Weight:166.22
Hs Code.:
DSSTox Substance ID:DTXSID90496574
Wikidata:Q82345539
Mol file:21681-63-0.mol

Synonyms:3-Cyclohexylideneoxolan-2-one;21681-63-0;DTXSID90496574;AKOS040803381

Suppliers and Price of 3-Cyclohexylideneoxolan-2-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 3-Cyclohexylideneoxolan-2-one

Chemical Property:

PSA：26.30000
LogP:2.19400
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:166.099379685
Heavy Atom Count:12
Complexity:220

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1CCC(=C2CCOC2=O)CC1

Technology Process of 3-Cyclohexylideneoxolan-2-one

There total 4 articles about 3-Cyclohexylideneoxolan-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 77772-24-8
α-(diphenylmethylsilyl)-γ-butyrolactone

: 21681-63-0
α-cyclohexylidene-γ-butyrolactone

Guidance literature:: With lithium diisopropyl amide; Yield given. Multistep reaction; 1.) THF, -78 deg C, 0.5 h, 2.) THF, reflux, 15 min;
DOI:10.1021/jo00225a052

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 66909-41-9
O-ethyl S-(tetrahydro-2-oxo-3-furanyl) thiocarbonate

: 21681-63-0
α-cyclohexylidene-γ-butyrolactone

Guidance literature:: With lithium diethylamide; Yield given. Multistep reaction; 1.) THF, -78 deg C, 1 h, 2.) THF, a.) -78 deg C, 2 h, b.) RT, 1 h;
DOI:10.1246/bcsj.53.2910