3-(Chloromethyl)-4-phenylfurazan 2-oxide

Base Information

Chemical Name:3-(Chloromethyl)-4-phenylfurazan 2-oxide
CAS No.:217966-10-4
Molecular Formula:C9H7ClN2O2
Molecular Weight:210.62
Hs Code.:
DSSTox Substance ID:DTXSID80434889
Nikkaji Number:J1.004.852D
Wikidata:Q82249471
ChEMBL ID:CHEMBL1631608

Synonyms:217966-10-4;3-(Chloromethyl)-4-phenylfurazan 2-oxide;CHEMBL1631608;DTXSID80434889;3-(Chloromethyl)-2-oxo-4-phenyl-1,2,5lambda~5~-oxadiazole

Suppliers and Price of 3-(Chloromethyl)-4-phenylfurazan 2-oxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 3-(Chloromethyl)-4-phenylfurazan 2-oxide

Chemical Property:

XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:2
Exact Mass:210.0196052
Heavy Atom Count:14
Complexity:188

Purity/Quality:: 97-99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C2=NO[N+](=C2CCl)[O-]

Technology Process of 3-(Chloromethyl)-4-phenylfurazan 2-oxide

There total 5 articles about 3-(Chloromethyl)-4-phenylfurazan 2-oxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 135733-30-1
3-(hydroxymethyl)-4-phenylfuroxan

: 217966-10-4
3-chloromethyl-4-phenyl-1,2,5-oxadiazole N²-oxide

Guidance literature:: With pyridine; thionyl chloride; In dichloromethane; at 20 ℃; Cooling with ice;

Reference yield:

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 217966-10-4
3-chloromethyl-4-phenyl-1,2,5-oxadiazole N²-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; sodium nitrite / water / 5 h / 20 °C

2: pyridine; thionyl chloride / dichloromethane / 20 °C

With pyridine; thionyl chloride; acetic acid; sodium nitrite; In dichloromethane; water;

Reference yield:

: 104-54-1
3-Phenylpropenol

: 217966-10-4
3-chloromethyl-4-phenyl-1,2,5-oxadiazole N²-oxide

Guidance literature:: Multi-step reaction with 2 steps

1: NaNO₂; AcOH

2: SOCl₂ / 20 °C

With thionyl chloride; acetic acid; sodium nitrite; 1: Cycloaddition / 2: Chlorination;
DOI:10.1021/jf9904766