5-(3,4-Dimethoxyphenyl)tetrazole-2-acetic acid (3-chlorobenzylidene)hydrazide

Base Information

Chemical Name:5-(3,4-Dimethoxyphenyl)tetrazole-2-acetic acid (3-chlorobenzylidene)hydrazide
CAS No.:94772-03-9
Molecular Formula:C₁₈H₁₇ClN₆O₃
Molecular Weight:400.824
Hs Code.:

Synonyms:BRN 4584579;5-(3,4-Dimethoxyphenyl)tetrazole-2-acetic acid (3-chlorobenzylidene)hydrazide;94772-03-9;2H-Tetrazole-2-acetic acid, 5-(3,4-dimethoxyphenyl)-, ((3-chlorophenyl)methylene)hydrazide;5-(3,4-Dimethoxyphenyl)-2H-tetrazole-2-acetic acid ((3-chlorophenyl)methylene)hydrazide

Suppliers and Price of 5-(3,4-Dimethoxyphenyl)tetrazole-2-acetic acid (3-chlorobenzylidene)hydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 5-(3,4-Dimethoxyphenyl)tetrazole-2-acetic acid (3-chlorobenzylidene)hydrazide

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:7
Exact Mass:400.1050661
Heavy Atom Count:28
Complexity:540

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=C(C=C(C=C1)C2=NN(N=N2)CC(=O)NN=CC3=CC(=CC=C3)Cl)OC
Isomeric SMILES:COC1=C(C=C(C=C1)C2=NN(N=N2)CC(=O)N/N=C/C3=CC(=CC=C3)Cl)OC

Technology Process of 5-(3,4-Dimethoxyphenyl)tetrazole-2-acetic acid (3-chlorobenzylidene)hydrazide

There total 4 articles about 5-(3,4-Dimethoxyphenyl)tetrazole-2-acetic acid (3-chlorobenzylidene)hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

: 94771-93-4
5-(3,4-Dimethoxyphenyl)tetrazole-2-acetic acid hydrazide

: 587-04-2
m-Chlorobenzaldehyde

: 94772-03-9
[5-(3,4-Dimethoxy-phenyl)-tetrazol-2-yl]-acetic acid [1-(3-chloro-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: With acetic acid; In ethanol; Heating;

Reference yield:

: 2024-83-1
veratronitrile

: 94772-03-9
[5-(3,4-Dimethoxy-phenyl)-tetrazol-2-yl]-acetic acid [1-(3-chloro-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 4 steps

1: 70 percent / NaN₃, NH₄Cl / dimethylformamide / 127 °C

2: 70 percent / NaOEt / ethanol / 16 h / Heating

3: 65 percent / 99percent H₂H₄*H₂O / ethanol / 8 h / Heating

4: 45 percent / AcOH / ethanol / Heating

With sodium azide; sodium ethanolate; ammonium chloride; hydrazine hydrate; acetic acid; In ethanol; N,N-dimethyl-formamide;

Reference yield:

: 10493-27-3
5-(3,4-Dimethoxyphenyl)tetrazole

: 94772-03-9
[5-(3,4-Dimethoxy-phenyl)-tetrazol-2-yl]-acetic acid [1-(3-chloro-phenyl)-meth-(E)-ylidene]-hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / NaOEt / ethanol / 16 h / Heating

2: 65 percent / 99percent H₂H₄*H₂O / ethanol / 8 h / Heating

3: 45 percent / AcOH / ethanol / Heating

With sodium ethanolate; hydrazine hydrate; acetic acid; In ethanol;