5-Chloro-3-[2-(5-chloro-2-methylthien-3-yl)cyclopent-1-en-1-yl]-2-methylthiophene

Base Information

Chemical Name:5-Chloro-3-[2-(5-chloro-2-methylthien-3-yl)cyclopent-1-en-1-yl]-2-methylthiophene
CAS No.:219537-97-0
Molecular Formula:C15H14Cl2S2
Molecular Weight:329.314
Hs Code.:29349990
DSSTox Substance ID:DTXSID201182451
Nikkaji Number:J1.018.049J
Mol file:219537-97-0.mol

Synonyms:219537-97-0;5-chloro-3-[2-(5-chloro-2-methylthien-3-yl)cyclopent-1-en-1-yl]-2-methylthiophene;1,2-Bis-(2-chloro-5-methylthien-4-yl)-cyclopentene;1,2-Bis(5-chloro-2-methylthiophen-3-yl)cyclopent-1-ene;5-chloro-3-[2-(5-chloro-2-methylthiophen-3-yl)cyclopent-1-en-1-yl]-2-methylthiophene;1,2-Bis(5-chloro-2-methyl-3-thienyl)cyclopentene;5-chloro-3-[2-(5-chloro-2-methylthiophen-3-yl)cyclopenten-1-yl]-2-methylthiophene;YSZC349;SCHEMBL4420882;DTXSID201182451;MFCD19382349;AKOS037646375;AS-68483;CS-0080091;EN300-81734;W15675;10.14272/DGZQNPCSQDROIH-UHFFFAOYSA-N.1;doi:10.14272/DGZQNPCSQDROIH-UHFFFAOYSA-N.1;3,3'-(1-Cyclopentene-1,2-diyl)bis[5-chloro-2-methylthiophene];3,3'-(cyclopent-1-ene-1,2-diyl)bis(5-chloro-2-methylthiophene)

Suppliers and Price of 5-Chloro-3-[2-(5-chloro-2-methylthien-3-yl)cyclopent-1-en-1-yl]-2-methylthiophene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 24 raw suppliers

Chemical Property of 5-Chloro-3-[2-(5-chloro-2-methylthien-3-yl)cyclopent-1-en-1-yl]-2-methylthiophene

Chemical Property:

Melting Point:76.1 - 78.2 °C
Boiling Point:436.8±45.0 °C(Predicted)
PSA：56.48000
Density:1.362±0.06 g/cm3(Predicted)
LogP:6.82790
XLogP3:6.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:327.9913982
Heavy Atom Count:19
Complexity:348

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C(C=C(S1)Cl)C2=C(CCC2)C3=C(SC(=C3)Cl)C

Technology Process of 5-Chloro-3-[2-(5-chloro-2-methylthien-3-yl)cyclopent-1-en-1-yl]-2-methylthiophene

There total 3 articles about 5-Chloro-3-[2-(5-chloro-2-methylthien-3-yl)cyclopent-1-en-1-yl]-2-methylthiophene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17249-82-0
2-chloro-5-methylthiophene

: 219537-97-0
1,2-bis(5-chloro-2-methylthien-3-yl)cyclopent-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: 48 percent / AlCl₃ / CS₂ / 2 h / 0 - 20 °C

2: 44 percent / Zn dust; TiCl₃*(THF)3 / 1 h / 40 °C

With aluminium trichloride; titanium trichloride tris(tetrahydrofuran); zinc; In carbon disulfide; 1: Friedel-Crafts acylation / 2: McMurry reaction;
DOI:10.1002/1099-0690(200301)2003:1<155::AID-EJOC155>3.0.CO;2-S

Reference yield:

: 17249-82-0
2-chloro-5-methylthiophene

: 219537-96-9
1,2-bis(2-methylthien-3-yl)cyclopentene

: 219537-97-0
1,2-bis(5-chloro-2-methylthien-3-yl)cyclopent-1-ene

Guidance literature:: Multi-step reaction with 2 steps

1: aluminum (III) chloride / dichloromethane / 3 h / 20 °C / Cooling with ice

2: titanium tetrachloride; zinc / tetrahydrofuran / 2 h / Reflux; Inert atmosphere

With aluminum (III) chloride; titanium tetrachloride; zinc; In tetrahydrofuran; dichloromethane; 1: |Friedel-Crafts Acylation / 2: |McMurry Reaction;
DOI:10.1002/poc.3584