Benzenemethanethiol, 3,5-bis[[3,5-bis(phenylmethoxy)phenyl]methoxy]-

Base Information

• Chemical Name: Benzenemethanethiol, 3,5-bis[[3,5-bis(phenylmethoxy)phenyl]methoxy]-
• CAS No.: 219657-44-0
• Molecular Formula: C49H44O6S
• Molecular Weight: 760.951
• Mol file: 219657-44-0.mol

Synonyms:

Chemical Property of Benzenemethanethiol, 3,5-bis[[3,5-bis(phenylmethoxy)phenyl]methoxy]-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Benzenemethanethiol, 3,5-bis[[3,5-bis(phenylmethoxy)phenyl]methoxy]-

There total 3 articles about Benzenemethanethiol, 3,5-bis[[3,5-bis(phenylmethoxy)phenyl]methoxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

3,5-bis[3,5-bis(benzyloxy)benzyloxy]benzyl bromide (129536-41-0) → [3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-phenyl]-methanethiol (219657-44-0)

Guidance literature:

With thiourea; In tetrahydrofuran; ethanol; at 79.84 ℃; for 4h; Inert atmosphere;

DOI:10.1039/d1cc05235g

Reference yield:

2-[3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-benzyl]-isothiourea → [3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-phenyl]-methanethiol (219657-44-0)

Guidance literature:

With hydrogenchloride; potassium hydroxide; for 4h; Heating;

DOI:10.1246/cl.1998.1197

Reference yield:

C51H46O7S → [3,5-bis-(3,5-bis-benzyloxy-benzyloxy)-phenyl]-methanethiol (219657-44-0)

Guidance literature:

DOI:10.1016/j.tetasy.2008.02.002

upstream raw materials:

3,5-bis[3,5-bis(benzyloxy)benzyloxy]benzyl bromide

Downstream raw materials:

C₇₃H₈₀N₂O₁₁S₃