1-Chloro-5-[(3-prop-1-en-2-ylcyclohexyl)methyl]naphthalene

Base Information

Chemical Name:1-Chloro-5-[(3-prop-1-en-2-ylcyclohexyl)methyl]naphthalene
CAS No.:5176-98-7
Molecular Formula:C₁₀H₁₇N₃
Molecular Weight:179.265
Hs Code.:
NSC Number:171453
DSSTox Substance ID:DTXSID30305676

Synonyms:5176-98-7;NSC171453;DTXSID30305676;1-chloro-5-[(3-prop-1-en-2-ylcyclohexyl)methyl]naphthalene;NSC-171453

Suppliers and Price of 1-Chloro-5-[(3-prop-1-en-2-ylcyclohexyl)methyl]naphthalene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 1-Chloro-5-[(3-prop-1-en-2-ylcyclohexyl)methyl]naphthalene

Chemical Property:

Vapor Pressure:8.62E-07mmHg at 25°C
Boiling Point:417.4°C at 760 mmHg
Flash Point:182.2°C
Density:1.081g/cm³
XLogP3:7.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:0
Rotatable Bond Count:3
Exact Mass:298.1488284
Heavy Atom Count:21
Complexity:361

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC(=C)C1CCCC(C1)CC2=C3C=CC=C(C3=CC=C2)Cl

Technology Process of 1-Chloro-5-[(3-prop-1-en-2-ylcyclohexyl)methyl]naphthalene

There total 2 articles about 1-Chloro-5-[(3-prop-1-en-2-ylcyclohexyl)methyl]naphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 462-69-1
N-butylguanidine

: 123-54-6,81235-32-7
acetylacetone

: 5176-98-7
2-(butylamino)-4,6-dimethylpyrimidine

Guidance literature:: for 0.0666667h; Microwave irradiation;
DOI:10.1246/bcsj.82.1175

Reference yield:

: 5176-98-7
2-(butylamino)-4,6-dimethylpyrimidine

Guidance literature:: 2-Chlor-4,6-dimethylpyrimidin, BuNH2 (98grad);

Reference yield:

: 5176-98-7
2-(butylamino)-4,6-dimethylpyrimidine

: Butyl-(4,6-dimethyl-pyrimidin-2-yl)-[2'-(2H-tetrazol-5-yl)-biphenyl-4-ylmethyl]-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) 1,3-dimethyl-3,4,5,6-tetrahydro-2-pyrimidinone, LiN(TMS)2 / 1.) THF, 0 deg C, 10 min, 2.) THF, RT, 90 min

2: 88percent aq. HCOOH / CH₂Cl₂ / 2 h / Ambient temperature

With 1,3-dimethyl-3,4,5,6-tetrahydro-2(1H)-pyrimidinone; formic acid; lithium hexamethyldisilazane; In dichloromethane;
DOI:10.1021/jm00070a012