Benzoic acid, 3-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene]amino]-4-[2-[[[(1, 1-dimethylethoxy)carbonyl]amino]methyl]-5-oxo-1-pyrrolidinyl]-, methyl ester

Base Information

Chemical Name:Benzoic acid, 3-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene]amino]-4-[2-[[[(1, 1-dimethylethoxy)carbonyl]amino]methyl]-5-oxo-1-pyrrolidinyl]-, methyl ester
CAS No.:221382-02-1
Molecular Formula:C29H43N5O9
Molecular Weight:605.689
Hs Code.:
Mol file:221382-02-1.mol

Benzoic acid,
3-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene]amino]-4-[2-[[[(1,
1-dimethylethoxy)carbonyl]amino]methyl]-5-oxo-1-pyrrolidinyl]-, methyl
ester

Synonyms:

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Chemical Property of Benzoic acid, 3-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene]amino]-4-[2-[[[(1, 1-dimethylethoxy)carbonyl]amino]methyl]-5-oxo-1-pyrrolidinyl]-, methyl ester

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Technology Process of Benzoic acid, 3-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene]amino]-4-[2-[[[(1, 1-dimethylethoxy)carbonyl]amino]methyl]-5-oxo-1-pyrrolidinyl]-, methyl ester

There total 7 articles about Benzoic acid, 3-[[bis[[(1,1-dimethylethoxy)carbonyl]amino]methylene]amino]-4-[2-[[[(1, 1-dimethylethoxy)carbonyl]amino]methyl]-5-oxo-1-pyrrolidinyl]-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 322474-21-5
N,N'-bis-Boc-S-methyl-isothiourea

: 221382-01-0
1-(4-methoxycarboxy-2-aminophenyl)-5-(tert-butyloxycarbonylaminomethyl)pyrrolidin-2-one

: 221382-02-1
1-<4-methoxycarbonyl-2-(N,N'-bis(tert-butyloxycarbonyl)guanidino)phenyl>-5-(tert-butyloxycarbonylaminomethyl)pyrrolidin-2-one

Guidance literature:: With triethylamine; mercury dichloride; In N,N-dimethyl-formamide; at 0 - 10 ℃; for 4h;
DOI:10.1021/jm980707k

Reference yield:

: 453-71-4
3-nitro-4-fluorobenzoic acid

: 221382-02-1
1-<4-methoxycarbonyl-2-(N,N'-bis(tert-butyloxycarbonyl)guanidino)phenyl>-5-(tert-butyloxycarbonylaminomethyl)pyrrolidin-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) DMF, 75 deg C, 15 min, 2.) DMF, RT, 20 h

2: 96 percent / H₂SO₄ / 12 h / Heating

3: 100 percent / H₂ / 10 percent Pd/C / ethyl acetate / 2.5 h / 1551.44 Torr

4: 60 percent / Et₃N, HgCl₂ / dimethylformamide / 4 h / 0 - 10 °C

With sulfuric acid; hydrogen; sodium hydride; triethylamine; mercury dichloride; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm980707k

Reference yield:

: 113466-82-3
5-(azidomethyl)-2-pyrrolidinone

: 221382-02-1
1-<4-methoxycarbonyl-2-(N,N'-bis(tert-butyloxycarbonyl)guanidino)phenyl>-5-(tert-butyloxycarbonylaminomethyl)pyrrolidin-2-one

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NaH / 1.) DMF, 75 deg C, 15 min, 2.) DMF, RT, 20 h

2: 96 percent / H₂SO₄ / 12 h / Heating

3: 100 percent / H₂ / 10 percent Pd/C / ethyl acetate / 2.5 h / 1551.44 Torr

4: 60 percent / Et₃N, HgCl₂ / dimethylformamide / 4 h / 0 - 10 °C

With sulfuric acid; hydrogen; sodium hydride; triethylamine; mercury dichloride; palladium on activated charcoal; In ethyl acetate; N,N-dimethyl-formamide;
DOI:10.1021/jm980707k