Nickel, dibromobis(diethylphenylphosphine)-

Base Information

Chemical Name:Nickel, dibromobis(diethylphenylphosphine)-
CAS No.:22330-25-2
Molecular Formula:C₂₀H₃₀Br₂NiP₂
Molecular Weight:550.904
Hs Code.:
Mol file:22330-25-2.mol

Synonyms:

Suppliers and Price of Nickel, dibromobis(diethylphenylphosphine)-

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Nickel, dibromobis(diethylphenylphosphine)-

Chemical Property:

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Technology Process of Nickel, dibromobis(diethylphenylphosphine)-

There total 1 articles about Nickel, dibromobis(diethylphenylphosphine)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1605-53-4
diethyl-phenyl-phosphine

: 13462-88-9
nickel dibromide

: 22330-25-2,69460-31-7,70492-63-6
Ni(II)Br₂(PEt₂Ph)2

Guidance literature:: In not given; prepd. from NiBr2 and PPhEt2 in 1-butanol or EtOH by method of R.G.Hayter and F.S.Humiec, Inorg. Chem., 4, 1701 (1965);
DOI:10.1246/bcsj.60.1589

Reference yield: 84.0%

: 22330-25-2,69460-31-7,70492-63-6
trans-dibromobis(diethylphenylphosphine)nickel(II)

: 2-ClC₆H₄Ni(P(C₂H₅)2C₆H₅)2Br

Guidance literature:: In tetrahydrofuran; benzene; byproducts: MgBr2; at -10 - -15 °C;; treatment with dild. HBr at -40 °C;;
DOI:10.1021/ja00709a012

Reference yield: 75.0%

: 22330-25-2,69460-31-7,70492-63-6
trans-dibromobis(diethylphenylphosphine)nickel(II)

: 61739-61-5
1-bromo-2-[4-(2-bromophenoxy)butoxy]benzene

: 61919-77-5
bis(diethylphenylphosphine)[2,2'-(tetramethylenedioxydiphenyl)]nickel(II)

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; benzene; stirring of ligand precursor (in THF) with BuLi (in hexane) for 15 min, addn. of suspn. of Ni-complex (in C6H6), stirring for 20 h; evapn., extn. into hot heptane, volume reduction (crystn.); elem. anal.;
DOI:10.1039/DT9760002053