Bullvalone

Base Information

Chemical Name:Bullvalone
CAS No.:15719-09-2
Molecular Formula:C₁₀H₁₀O
Molecular Weight:146.189
Hs Code.:
DSSTox Substance ID:DTXSID20481337
Nikkaji Number:J55.586J
Mol file:15719-09-2.mol

Synonyms:15719-09-2;Tricyclo[3.3.2.02,8]deca-6,9-dien-3-one;Bullvalone;Tricyclo[3.3.2.0~2,8~]deca-6,9-dien-3-one;DTXSID20481337

Suppliers and Price of Bullvalone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Bullvalone

Chemical Property:

Boiling Point:265.1±9.0 °C(Predicted)
PSA：17.07000
Density:1.193±0.06 g/cm3(Predicted)
LogP:1.56360
XLogP3:1.1
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:0
Exact Mass:146.073164938
Heavy Atom Count:11
Complexity:255

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2C=CC3C(C3C1=O)C=C2

Technology Process of Bullvalone

There total 8 articles about Bullvalone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

: 6006-24-2
tricyclo<3.3.1.0^2,8>nona-3,6-dien-9-one

: 18107-18-1
diazomethyl-trimethyl-silane

: 15719-09-2
tricyclo[3.3.2.0^2,8]deca-6,9-dien-4-one

Guidance literature:: tricyclo<3.3.1.0^2,8>nona-3,6-dien-9-one; With n-butyllithium; In diethyl ether; at -78 ℃; Inert atmosphere; Schlenk technique;

diazomethyl-trimethyl-silane; In tetrahydrofuran; diethyl ether; at -78 ℃; for 0.5h; Inert atmosphere; Schlenk technique;
DOI:10.1002/anie.201606101

Reference yield:

: 34733-74-9
bicyclo[4.2.1]nona-2,4,7-trien-9-one

: 15719-09-2
tricyclo[3.3.2.0^2,8]deca-6,9-dien-4-one

Guidance literature:: Multi-step reaction with 2 steps

1: 4,4'-bis-dimethylamino-benzophenone / Irradiation

2: methanol

With bis(p-dimethylaminophenyl)methanone; In methanol;
DOI:10.1021/jo00905a007