8,8-Dimethyl-2-oxaspiro[4.5]decane-1,3-dione

Base Information

Chemical Name:8,8-Dimethyl-2-oxaspiro[4.5]decane-1,3-dione
CAS No.:51111-15-0
Molecular Formula:C₁₁H₁₆O₃
Molecular Weight:196.246
Hs Code.:
NSC Number:159450
DSSTox Substance ID:DTXSID30303632
Wikidata:Q82049011
Mol file:51111-15-0.mol

Synonyms:8,8-dimethyl-2-oxaspiro[4.5]decane-1,3-dione;51111-15-0;NSC159450;SCHEMBL8868873;DTXSID30303632;AKOS013741341;NSC-159450

Suppliers and Price of 8,8-Dimethyl-2-oxaspiro[4.5]decane-1,3-dione

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 8,8-Dimethyl-2-oxaspiro[4.5]decane-1,3-dione

Chemical Property:

Vapor Pressure:0.00032mmHg at 25°C
Boiling Point:320.3°Cat760mmHg
Flash Point:146.5°C
Density:1.12g/cm³
XLogP3:2.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:0
Exact Mass:196.109944368
Heavy Atom Count:14
Complexity:281

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1(CCC2(CC1)CC(=O)OC2=O)C

Technology Process of 8,8-Dimethyl-2-oxaspiro[4.5]decane-1,3-dione

There total 10 articles about 8,8-Dimethyl-2-oxaspiro[4.5]decane-1,3-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 39858-62-3
cyano-(4,4-dimethyl-cyclohexyliden)-acetic acid ethyl ester

: 51111-15-0
8,8-dimethyl-2-oxa-spiro[4.5]decane-1,3-dione

Guidance literature:: Multi-step reaction with 3 steps

1: ethanol; H₂O / 5 h / Heating

2: acetic acid, HCl, H₂O / 84 h / Heating

3: acetic anhydride / 4 h / Heating

With hydrogenchloride; water; acetic anhydride; acetic acid; In ethanol; water;
DOI:10.1021/jm00173a010

Reference yield:

: 4255-62-3
4,4-dimethylcyclohexane-1-one

: 51111-15-0
8,8-dimethyl-2-oxa-spiro[4.5]decane-1,3-dione

Guidance literature:: Multi-step reaction with 4 steps

1: ammonium acetate, acetic acid / toluene / Heating

2: ethanol; H₂O / 5 h / Heating

3: acetic acid, HCl, H₂O / 84 h / Heating

4: acetic anhydride / 4 h / Heating

With ammonium acetate; hydrogenchloride; water; acetic anhydride; acetic acid; In ethanol; water; toluene;
DOI:10.1021/jm00173a010