Dinitrosodiphenylparaphenylendiamin

Base Information

• Chemical Name: Dinitrosodiphenylparaphenylendiamin
• CAS No.: 2716-09-8
• Molecular Formula: C18H14 N4 O2
• Molecular Weight: 0
• NSC Number: 56932
• DSSTox Substance ID: DTXSID80949908
• Wikidata: Q82927859
• Mol file: 2716-09-8.mol

Synonyms:2716-09-8;NSC56932;SCHEMBL9292268;Dinitrosodiphenylparaphenylendiamin;DTXSID80949908;NSC-56932;N,N'-1,4-Phenylenebis(N-phenylnitrous amide)

Chemical Property of Dinitrosodiphenylparaphenylendiamin

Chemical Property:

• Boiling Point: 560.8oC at 760 mmHg
• Flash Point: 292.9oC
• PSA: 65.34000
• Density: 1.21g/cm3
• LogP: 5.32560
• XLogP3: 4.5
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 6
• Rotatable Bond Count: 4
• Exact Mass: 318.11167570
• Heavy Atom Count: 24
• Complexity: 362

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)N(C2=CC=C(C=C2)N(C3=CC=CC=C3)N=O)N=O

Technology Process of Dinitrosodiphenylparaphenylendiamin

There total 4 articles about Dinitrosodiphenylparaphenylendiamin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

N,N'-diphenyl-1,4-phenylenediamine (74-31-7,943443-44-5) → N,N'-dinitroso-N,N'-diphenyl-p-phenylenediamine (2716-09-8)

Guidance literature:

With trichloromelamine; silica gel; sodium nitrite; In dichloromethane; water; at 20 ℃; for 0.416667h;

DOI:10.1134/S1070428007090229

Reference yield: 20.0%

N,N'-diphenyl-1,4-phenylenediamine (74-31-7,943443-44-5) → C18H15N3O + N,N'-dinitroso-N,N'-diphenyl-p-phenylenediamine (2716-09-8)

Guidance literature:

With trichloromelamine; silica gel; sodium nitrite; In dichloromethane; water; at 20 ℃; for 0.5h;

DOI:10.1134/S1070428007090229

Reference yield:

→ N,N'-dinitroso-N,N'-diphenyl-p-phenylenediamine (2716-09-8)

Guidance literature:

With acetic acid; sodium nitrite;

upstream raw materials:

ethanol

N,N'-diphenyl-1,4-phenylenediamine

N,N'-diphenyl-1,4-phenylenediamine

Downstream raw materials:

N,N'-diphenyl-1,4-phenylenediamine