Benzenamine, 2,2'-dithiobis[5-fluoro-

Base Information

Chemical Name:Benzenamine, 2,2'-dithiobis[5-fluoro-
CAS No.:224791-45-1
Molecular Formula:C12H10F2N2S2
Molecular Weight:284.354
Hs Code.:
DSSTox Substance ID:DTXSID90444136
Wikidata:Q82262164
Mol file:224791-45-1.mol

Synonyms:Benzenamine, 2,2'-dithiobis[5-fluoro-;224791-45-1;SCHEMBL4808061;DTXSID90444136

Suppliers and Price of Benzenamine, 2,2'-dithiobis[5-fluoro-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of Benzenamine, 2,2'-dithiobis[5-fluoro-

Chemical Property:

Melting Point:75-76 °C
Boiling Point:405.6±45.0 °C(Predicted)
PSA：102.64000
Density:1.46±0.1 g/cm3(Predicted)
LogP:5.09100
XLogP3:2.9
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:284.02534700
Heavy Atom Count:18
Complexity:245

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=C(C=C1F)N)SSC2=C(C=C(C=C2)F)N

Technology Process of Benzenamine, 2,2'-dithiobis[5-fluoro-

There total 4 articles about Benzenamine, 2,2'-dithiobis[5-fluoro- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 20358-07-0
2-amino-5-fluorobenzothiazole

: 224791-45-1
4,4'-difluoro-2,2'-diaminodiphenyl disulfide

Guidance literature:: With potassium hydroxide; for 5h; Heating;
DOI:10.1021/jm001104n

Reference yield: 13.0%

: 6-fluoro-1,3λ⁴δ²,2,4-benzodithiadiazine

: 224791-45-1
4,4'-difluoro-2,2'-diaminodiphenyl disulfide

Guidance literature:: With water; at 20 ℃; for 720h;
DOI:10.1070/MC2003v013n01ABEH001700

Reference yield:

: 372-19-0
meta-fluoroaniline

: 224791-45-1
4,4'-difluoro-2,2'-diaminodiphenyl disulfide

Guidance literature:: Multi-step reaction with 3 steps

1.1: benzoyl chloride / acetone / 1 h / Heating

1.2: 91 percent / aq. NaOH / 1.5 h / Heating

2.1: 64 percent / bromine / CH₂Cl₂ / 3 h / Heating

3.1: 76 percent / aq. potassium hydroxide / 5 h / Heating

With potassium hydroxide; bromine; benzoyl chloride; In dichloromethane; acetone;
DOI:10.1016/j.bmc.2006.08.026