6-methoxy-3-isoquinolinecarboxylic acid ethyl ester picrate

Base Information

• Chemical Name: 6-methoxy-3-isoquinolinecarboxylic acid ethyl ester picrate
• CAS No.: 86804-63-9
• Molecular Formula: C₆H₃N₃O₇*C₁₃H₁₃NO₃
• Molecular Weight: 460.357
• Mol file: 86804-63-9.mol

Synonyms:

Chemical Property of 6-methoxy-3-isoquinolinecarboxylic acid ethyl ester picrate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 6-methoxy-3-isoquinolinecarboxylic acid ethyl ester picrate

There total 1 articles about 6-methoxy-3-isoquinolinecarboxylic acid ethyl ester picrate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

ethanol (64-17-5) + 6-methoxy-1,2,3,4-tetrahydro-isoquinoline-3-carboxylic acid (77140-86-4) + 2,4,6-Trinitrophenol (88-89-1) → 6-methoxy-3-isoquinolinecarboxylic acid ethyl ester picrate (86804-63-9)

Guidance literature:

With thionyl chloride; Yield given. Multistep reaction; 1.) reflux, 1 h, 2.) overnight;

upstream raw materials:

ethanol

6-methoxy-1,2,3,4-tetrahydro-isoquinoline-3-carboxylic acid

2,4,6-Trinitrophenol