2,2'-Bipyridine, 4-(4-bromophenyl)-

Base Information

Chemical Name:2,2'-Bipyridine, 4-(4-bromophenyl)-
CAS No.:225669-83-0
Molecular Formula:C16H11BrN2
Molecular Weight:311.181
Hs Code.:
DSSTox Substance ID:DTXSID00464542
Nikkaji Number:J1.780.789G
Wikidata:Q82289907
Mol file:225669-83-0.mol

Synonyms:2,2'-Bipyridine, 4-(4-bromophenyl)-;225669-83-0;4-(4-bromophenyl)-2-pyridin-2-ylpyridine;4-(4-Bromophenyl)-2,2'-bipyridine;DTXSID00464542;J-400385

Suppliers and Price of 2,2'-Bipyridine, 4-(4-bromophenyl)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 2,2'-Bipyridine, 4-(4-bromophenyl)-

Chemical Property:

XLogP3:3.8
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:310.01056
Heavy Atom Count:19
Complexity:276

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=NC(=C1)C2=NC=CC(=C2)C3=CC=C(C=C3)Br

Technology Process of 2,2'-Bipyridine, 4-(4-bromophenyl)-

There total 5 articles about 2,2'-Bipyridine, 4-(4-bromophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

: 257620-49-8
4-(4-bromophenyl)-6-(pyridin-2-yl)pyridine-2-carboxylic acid

: 225669-83-0
4-(4-bromo)phenyl-2,2’-bipyridine

Guidance literature:: In diethylene glycol; Heating;
DOI:10.2533/000942903777679569

Reference yield: 41.0%

: 477566-82-8
2-[4-(4-bromo-phenyl)-6-ethoxy-5,6-dihydro-4H-pyran-2-yl]-pyridine

: 225669-83-0
4-(4-bromo)phenyl-2,2’-bipyridine

Guidance literature:: With hydroxylamine hydrochloride; In acetonitrile; for 6h; Heating;
DOI:10.1039/b203595b

Reference yield:

: 1122-62-9
2-acetylpyridine

: 225669-83-0
4-(4-bromo)phenyl-2,2’-bipyridine

Guidance literature:: Multi-step reaction with 3 steps

1: 66 percent / aq. NaOH / methanol / 20 °C

2: 91 percent / yttrium(III) hexafluoroacetylacetonate / tetrahydrofuran / 20 °C

3: 41 percent / NH₂OH*HCl / acetonitrile / 6 h / Heating

With sodium hydroxide; hydroxylamine hydrochloride; yttrium(III) hexafluoroacetylacetonate; In tetrahydrofuran; methanol; acetonitrile;
DOI:10.1039/b203595b