N-[9-((R)-1-{(R)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-2-hydroxy-ethyl)-9H-purin-6-yl]-benzamide

Base Information

• Chemical Name: N-[9-((R)-1-{(R)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-2-hydroxy-ethyl)-9H-purin-6-yl]-benzamide
• CAS No.: 98815-85-1
• Molecular Formula: C₄₃H₄₉N₅O₆Si
• Molecular Weight: 759.977

Synonyms:

Chemical Property of N-[9-((R)-1-{(R)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-2-hydroxy-ethyl)-9H-purin-6-yl]-benzamide

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Technology Process of N-[9-((R)-1-{(R)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-2-hydroxy-ethyl)-9H-purin-6-yl]-benzamide

There total 1 articles about N-[9-((R)-1-{(R)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-2-hydroxy-ethyl)-9H-purin-6-yl]-benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

N-[9-((R)-2-Hydroxy-1-{(S)-1-hydroxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-ethyl)-9H-purin-6-yl]-benzamide (98815-82-8) + tert-butyldimethylsilyl chloride (18162-48-6) → N-[9-((R)-1-{(R)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-2-hydroxy-ethyl)-9H-purin-6-yl]-benzamide (98815-85-1) + N-[9-((R)-2-(tert-Butyl-dimethyl-silanyloxy)-1-{(S)-1-hydroxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-ethyl)-9H-purin-6-yl]-benzamide (98815-84-0) + N-[9-((R)-2-(tert-Butyl-dimethyl-silanyloxy)-1-{(R)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-ethyl)-9H-purin-6-yl]-benzamide (98815-83-9)

Guidance literature:

In pyridine;

DOI:10.1016/S0040-4039(00)94778-6

Reference yield:

N-[9-((R)-1-{(R)-1-(tert-Butyl-dimethyl-silanyloxymethyl)-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-2-hydroxy-ethyl)-9H-purin-6-yl]-benzamide (98815-85-1) → Benzoic acid (R)-2-(6-benzoylamino-purin-9-yl)-2-{(R)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-ethyl ester (98815-87-3)

Guidance literature:

DOI:10.1016/S0040-4039(00)94778-6

upstream raw materials:

N-[9-((R)-2-Hydroxy-1-{(S)-1-hydroxymethyl-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-ethyl)-9H-purin-6-yl]-benzamide

tert-butyldimethylsilyl chloride

Downstream raw materials:

Benzoic acid (R)-2-(6-benzoylamino-purin-9-yl)-2-{(R)-1-(tert-butyl-dimethyl-silanyloxymethyl)-2-[(4-methoxy-phenyl)-diphenyl-methoxy]-ethoxy}-ethyl ester

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