4-[(4-bromophenyl)diazenyl]-N,N-diethylaniline

Base Information

Chemical Name:4-[(4-bromophenyl)diazenyl]-N,N-diethylaniline
CAS No.:22700-62-5
Molecular Formula:C16H18BrN3
Molecular Weight:332.243
Hs Code.:
European Community (EC) Number:660-445-7
DSSTox Substance ID:DTXSID201037533
Nikkaji Number:J1.056.862E

Synonyms:4-[(4-bromophenyl)diazenyl]-N,N-diethylaniline;22700-62-5;4'-Bromo-4-(diethylamino)azobenzene;N1,N1-diethyl-4-[2-(4-bromophenyl)diaz-1-enyl]aniline;SCHEMBL17279183;CHEBI:192643;DTXSID201037533;4-[(E)-(4-bromophenyl)diazenyl]-N,N-diethylaniline

Suppliers and Price of 4-[(4-bromophenyl)diazenyl]-N,N-diethylaniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 4-[(4-bromophenyl)diazenyl]-N,N-diethylaniline

Chemical Property:

XLogP3:5.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:5
Exact Mass:331.06841
Heavy Atom Count:20
Complexity:288

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCN(CC)C1=CC=C(C=C1)N=NC2=CC=C(C=C2)Br

Technology Process of 4-[(4-bromophenyl)diazenyl]-N,N-diethylaniline

There total 3 articles about 4-[(4-bromophenyl)diazenyl]-N,N-diethylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 106-40-1
4-bromo-aniline

: 91-66-7
N,N-diethylaniline

: 22700-62-5
(E)-4-((4-bromophenyl)diazenyl)-N,N-diethylaniline

Guidance literature:: 4-bromo-aniline; With hydrogenchloride; sodium nitrite; In water; at 0 ℃; for 0.5h;

N,N-diethylaniline; With sodium acetate; In methanol; water; at 0 - 5 ℃; for 2h;
DOI:10.1039/c8nj01346b

Reference yield: 84.0%

: 673-40-5
4-bromobenzenediazonium tetrafluoroborate

: 91-66-7
N,N-diethylaniline

: 22700-62-5
(E)-4-((4-bromophenyl)diazenyl)-N,N-diethylaniline

Guidance literature:: With Eosin Y; In acetonitrile; at 20 ℃; for 2h; Irradiation; Schlenk technique;
DOI:10.1002/chem.201905308

Reference yield:

: 106-40-1
4-bromo-aniline

: 91-66-7
N,N-diethylaniline

: 22700-62-5
4-Diethylamino-4'-bromo-azobenzen

Guidance literature:: With hydrogenchloride; sodium acetate; sodium nitrite; Multistep reaction; 1.) H₂O, 0 deg C, 10 min, 2.) aq. CH₃COOH, 2 h, 0-5 deg C;