tert-butyl β-(tri-n-butylstannyl)-α-benzyl-propionate

Base Information

Chemical Name:tert-butyl β-(tri-n-butylstannyl)-α-benzyl-propionate
CAS No.:118666-11-8
Molecular Formula:C₂₆H₄₆O₂Sn
Molecular Weight:509.36
Hs Code.:

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Chemical Property of tert-butyl β-(tri-n-butylstannyl)-α-benzyl-propionate

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Technology Process of tert-butyl β-(tri-n-butylstannyl)-α-benzyl-propionate

There total 1 articles about tert-butyl β-(tri-n-butylstannyl)-α-benzyl-propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 16537-10-3
tert-butyl 3-phenylpropanoate

: 4111-55-1
lithium dicyclohexylamide

: 66222-29-5
tri-n-butylstannylmethyl iodide

: 118666-11-8
tert-butyl β-(tri-n-butylstannyl)-α-benzyl-propionate

Guidance literature:: In tetrahydrofuran; ligand in hexane was treated with lithium dicyclohexylamide in THF at -78°C for 30 min, Sn-complex in THF was added under N2, the mixt. was slowly warmed to room temp., poured into aq. citric acid, extd. with petroleun ether; organic extracts were washed with aq. citric acid, H2O, sodium bicarbonate, H2O, dried with sodium sulphate, evapd., crude ppt. was purified by column chromy. on silica gel, using petroleum ether and CH2Cl2 as eluant;