1-Phenyl-3-(triethylsiloxy)propane

Base Information

• Chemical Name: 1-Phenyl-3-(triethylsiloxy)propane
• CAS No.: 2290-40-6
• Molecular Formula: C15H26OSi
• Molecular Weight: 250.456
• Hs Code.: 2931900090
• Mol file: 2290-40-6.mol

Synonyms:3-phenylpropyl triethylsilyl ether;hydrocinnamyl triethylsilyl ether;3-Phenylpropanol triethylsilyl ether;

Chemical Property of 1-Phenyl-3-(triethylsiloxy)propane

Chemical Property:

• PSA: 9.23000
• LogP: 4.64100

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-Phenyl-3-(triethylsiloxy)propane

There total 33 articles about 1-Phenyl-3-(triethylsiloxy)propane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

triethylsilane (617-86-7) + 3-Phenyl-1-propanol (122-97-4) → 3-phenylpropanol triethylsilyl ether (2290-40-6)

Guidance literature:

With C₄₂H₄₆F₆N₂O₆PRh₂⁽¹⁺⁾*F₆Sb^(1-); In dichloromethane; at 20 ℃; for 1h; Inert atmosphere; Schlenk technique; Sealed tube;

DOI:10.1021/acs.organomet.1c00314

Reference yield: 97.2%

triethylsilyl chloride (994-30-9) + 3-phenyl-1-propanol formate ester (104-64-3) → 3-phenylpropanol triethylsilyl ether (2290-40-6)

Guidance literature:

With samarium diiodide; In tetrahydrofuran; N,N,N,N,N,N-hexamethylphosphoric triamide; at 20 ℃; for 0.0833333h;

DOI:10.1080/00397919908085960

Reference yield: 94.0%

1-(triethylsilyl)oxy-3-phenyl-2-propene (129541-12-4) → 3-phenylpropanol triethylsilyl ether (2290-40-6)

Guidance literature:

With hydrogen; In methanol; at 20 ℃; for 24h; under 760.051 Torr; Reagent/catalyst; chemoselective reaction;

DOI:10.1016/j.tet.2015.03.086

upstream raw materials:

3-phenyl-propionaldehyde

triethylsilane

3-Phenylpropenol

triethylsilyl chloride

Downstream raw materials:

3-Phenyl-1-propanol

2-(3-phenylpropoxy)tetrahydro-2H-pyran

((3-phenylpropoxy)methylene)dibenzene

1-benzyloxy-3-phenylpropane