bis[4,6-bis(trifluoromethyl)-2-(4-trifluoromethyl-2-pyridinyl-κN)phenyl-κC][bisphenylpyridine]iridium pentane

Base Information

• Chemical Name: bis[4,6-bis(trifluoromethyl)-2-(4-trifluoromethyl-2-pyridinyl-κN)phenyl-κC][bisphenylpyridine]iridium pentane
• CAS No.: 897937-59-6
• Molecular Formula: C₅H₁₂*C₅₆H₁₉F₃₆IrN₄
• Molecular Weight: 1696.11

Synonyms:

Chemical Property of bis[4,6-bis(trifluoromethyl)-2-(4-trifluoromethyl-2-pyridinyl-κN)phenyl-κC][bisphenylpyridine]iridium pentane

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Technology Process of bis[4,6-bis(trifluoromethyl)-2-(4-trifluoromethyl-2-pyridinyl-κN)phenyl-κC][bisphenylpyridine]iridium pentane

There total 1 articles about bis[4,6-bis(trifluoromethyl)-2-(4-trifluoromethyl-2-pyridinyl-κN)phenyl-κC][bisphenylpyridine]iridium pentane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.8%

2-[3,5-bis(trifluoromethyl)phenyl]-4-trifluoromethylpyridine + iridium(III) chloride trihydrate + silver trifluoroacetate (2966-50-9) → 2NC5H3(CF3)C6H3(CF3)2*3Ag(1+)*3O2CCF3(1-)=[Ag3(NC5H3(CF3)C6H3(CF3)2)2(O2CCF3)3] + tris[4,6-bis(trifluoromethyl)-2-(4-trifluoromethyl-2-pyridinyl-κN)phenyl-κC]iridium + bis[4,6-bis(trifluoromethyl)-2-(4-trifluoromethyl-2-pyridinyl-κN)phenyl-κC][bisphenylpyridine]iridium pentane (897937-59-6)

Guidance literature:

In water; byproducts: (CF3)2C6H3(CF3)C5H2NC6H2(CF3)2C5H2(CF3)N, CF3CO2H; (Ar); std. Schlenk technique; mixt. of ligand, Ir compd. and Ag salt in H2O was stirred at room temp. for 12 h; heated to 180°C during 10h; volatiles removed by flow of N2; heated for 48 h at 180°C; cooled to ambint temp.; dissolved in CH2Cl2; filtered; concd.; kept at room temp. for 12 h; chromd. (silica gel, petroleum ether/Et2O, 10/1); elem. anal.;

DOI:10.1039/b514797b

upstream raw materials:

silver trifluoroacetate

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