2H-Pyran-2-carboxylic acid, 3,4-dihydro-, methyl ester

Base Information

Chemical Name:2H-Pyran-2-carboxylic acid, 3,4-dihydro-, methyl ester
CAS No.:23125-70-4
Molecular Formula:C7H10O3
Molecular Weight:142.155
Hs Code.:
Mol file:23125-70-4.mol

Synonyms:

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Chemical Property of 2H-Pyran-2-carboxylic acid, 3,4-dihydro-, methyl ester

Chemical Property:

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Technology Process of 2H-Pyran-2-carboxylic acid, 3,4-dihydro-, methyl ester

There total 1 articles about 2H-Pyran-2-carboxylic acid, 3,4-dihydro-, methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 107-02-8,25068-14-8
acrolein

: 100-73-2
acrolein dimer

: 23125-70-4
2-(methoxycarbonyl)-3,4-dihydro-2H-pyran

Guidance literature:: With hydroquinone; In benzene; at 170 ℃; for 3h; Title compound not separated from byproducts;
DOI:10.1080/00397910008087136

Reference yield: 96.0%

: 23125-70-4
2-(methoxycarbonyl)-3,4-dihydro-2H-pyran

: 100-46-9
benzylamine

: 3,4-Dihydro-2H-pyran-2-carboxylic acid benzylamide

Guidance literature:: With lipase from Candida antarctica; In various solvent(s);
DOI:10.1016/0040-4039(95)00969-J

Reference yield:

: 23125-70-4
2-(methoxycarbonyl)-3,4-dihydro-2H-pyran

: 20781-20-8
2,4-Dimethoxybenzylamine

: (S)-3,4-Dihydro-2H-pyran-2-carboxylic acid 2,4-dimethoxy-benzylamide

: (R)-3,4-Dihydro-2H-pyran-2-carboxylic acid 2,4-dimethoxy-benzylamide

Guidance literature:: With lipase AY₃₀ from Candida cylindracea; In tetrachloromethane; at 25 ℃; for 48h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
DOI:10.1016/0040-4039(95)00969-J