2-Propyn-1-one, 1-(4-bromophenyl)-3-phenyl-

Base Information

Chemical Name:2-Propyn-1-one, 1-(4-bromophenyl)-3-phenyl-
CAS No.:23565-63-1
Molecular Formula:C15H9BrO
Molecular Weight:285.14
Hs Code.:
DSSTox Substance ID:DTXSID40462769
Nikkaji Number:J1.551.800F
Wikidata:Q82287356

Synonyms:2-Propyn-1-one, 1-(4-bromophenyl)-3-phenyl-;23565-63-1;SCHEMBL9194059;DTXSID40462769;1-(4-bromophenyl)-3-phenyl-2-propyn-1-one;InChI=1/C15H9BrO/c16-14-9-7-13(8-10-14)15(17)11-6-12-4-2-1-3-5-12/h1-5,7-10

Suppliers and Price of 2-Propyn-1-one, 1-(4-bromophenyl)-3-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 1 raw suppliers

Chemical Property of 2-Propyn-1-one, 1-(4-bromophenyl)-3-phenyl-

Chemical Property:

XLogP3:4.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:283.98368
Heavy Atom Count:17
Complexity:321

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)C#CC(=O)C2=CC=C(C=C2)Br

Technology Process of 2-Propyn-1-one, 1-(4-bromophenyl)-3-phenyl-

There total 34 articles about 2-Propyn-1-one, 1-(4-bromophenyl)-3-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 536-74-3
phenylacetylene

: 586-75-4
4-chlorobenzoyl chloride

: 23565-63-1
1-(4-bromophenyl)-3-phenylpropynone

Guidance literature:: phenylacetylene; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 1h; Inert atmosphere;

With morpholine; In tetrahydrofuran; hexane; at 0 ℃; for 0.5h; Inert atmosphere;

4-chlorobenzoyl chloride; In tetrahydrofuran; hexane; at 0 ℃; for 0.166667h; Inert atmosphere;
DOI:10.1002/bkcs.11450

Reference yield: 92.0%

: 201230-82-2
carbon monoxide

: 589-87-7
1,4-bromoiodobenzene

: 536-74-3
phenylacetylene

: 23565-63-1
1-(4-bromophenyl)-3-phenylpropynone

Guidance literature:: With triethylamine; In water; at 130 ℃; for 6h; under 22502.3 Torr; Autoclave;
DOI:10.1016/j.tetlet.2011.01.095

Reference yield: 91.0%

: 142739-40-0
1-(4-bromo-phenyl)-3-phenyl-prop-2-yn-1-ol

: 23565-63-1
1-(4-bromophenyl)-3-phenylpropynone

Guidance literature:: 1-(4-bromo-phenyl)-3-phenyl-prop-2-yn-1-ol; With oxalyl dichloride; dimethyl sulfoxide; In dichloromethane; at -78 ℃; for 0.25h; Inert atmosphere;

With triethylamine; In dichloromethane; at -78 - 21 ℃; for 1h; Inert atmosphere;
DOI:10.1039/c7ob02406a