(1S,18²S,18³S)-18²-(4-methoxy-phenyl)-2,6,6-trimethyl-16,19-dioxo-18^2,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphanium; chloride

Base Information

• Chemical Name: (1S,18²S,18³S)-18²-(4-methoxy-phenyl)-2,6,6-trimethyl-16,19-dioxo-18^2,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphanium; chloride
• CAS No.: 69721-95-5
• Molecular Formula: C₃₂H₄₅N₄O₄*Cl
• Molecular Weight: 585.187

Synonyms:

Chemical Property of (1S,18²S,18³S)-18²-(4-methoxy-phenyl)-2,6,6-trimethyl-16,19-dioxo-18^2,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphanium; chloride

Chemical Property:

Purity/Quality:

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Useful:

Technology Process of (1S,18²S,18³S)-18²-(4-methoxy-phenyl)-2,6,6-trimethyl-16,19-dioxo-18^2,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphanium; chloride

There total 1 articles about (1S,18²S,18³S)-18²-(4-methoxy-phenyl)-2,6,6-trimethyl-16,19-dioxo-18^2,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphanium; chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(1S,182S,183S)-182-(4-hydroxy-phenyl)-182,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphane-16,19-dione (75363-58-5) + methyl iodide (74-88-4) → (1S,182S,183S)-182-(4-methoxy-phenyl)-2,6,6-trimethyl-16,19-dioxo-182,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphanium; chloride (69721-95-5)

Guidance literature:

Multistep reaction; (i) K2CO3, MeOH, (ii) ion-exchange resin - form>;

DOI:10.1002/hlca.19780610735

upstream raw materials:

(1S,18²S,18³S)-18²-(4-hydroxy-phenyl)-18^2,3-dihydro-2,6,11,15-tetraaza-18(5,3)-benzofurana-bicyclo[9.6.2]nonadecaphane-16,19-dione

methyl iodide

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