3-Phenyl-2H-azirine-2-carboxylic acid ethyl ester

Base Information

• Chemical Name: 3-Phenyl-2H-azirine-2-carboxylic acid ethyl ester
• CAS No.: 23893-63-2
• Molecular Formula: C11H11NO2
• Molecular Weight: 189.214
• Hs Code.: 2933990090
• Mol file: 23893-63-2.mol

Synonyms:3-Phenyl-2H-azirin-2-carbonsaeureethylester;Ethyl-2-phenyl-1-azirin-3-carboxylat;3-phenyl-2H-azirine-2-carboxylic acid ethyl ester;2-phenyl-3-carbethoxyazirine;

Chemical Property of 3-Phenyl-2H-azirine-2-carboxylic acid ethyl ester

Chemical Property:

• PSA: 38.66000
• LogP: 0.85660

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

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MSDS Files:

SDS file from LookChem

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Technology Process of 3-Phenyl-2H-azirine-2-carboxylic acid ethyl ester

There total 8 articles about 3-Phenyl-2H-azirine-2-carboxylic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 37.0%

ethyl 2-bromo-3-phenyl-2H-azirine-2-carboxylate (221171-91-1) → ethyl 2-phenyl-2H-azirine-3-carboxylate (107973-65-9) + ethyl 3-phenyl-2H-azirine-2-carboxylate (23893-63-2) + ethyl 2-phenylaziridine-3-carboxylate (554450-49-6)

Guidance literature:

With sodium tetrahydroborate; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

DOI:10.1016/S0040-4020(03)00248-5

Reference yield: 28.0%

ethyl 2-chloro-3-phenyl-2H-azirine-2-carboxylate (221171-90-0) → ethyl 2-phenyl-2H-azirine-3-carboxylate (107973-65-9) + ethyl 3-phenyl-2H-azirine-2-carboxylate (23893-63-2)

Guidance literature:

With sodium tetrahydroborate; In N,N-dimethyl-formamide; at 50 ℃; for 0.25h;

DOI:10.1016/S0040-4020(03)00248-5

Reference yield: 27.0%

ethyl 2-chloro-3-phenyl-2H-azirine-2-carboxylate (221171-90-0) → ethyl 3-phenyl-2H-azirine-2-carboxylate (23893-63-2) + ethyl 2-phenylaziridine-3-carboxylate (554450-49-6)

Guidance literature:

With sodium tetrahydroborate; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

DOI:10.1016/S0040-4020(03)00248-5

upstream raw materials:

ethyl 2-bromo-3-phenyl-2H-azirine-2-carboxylate

ethyl 2-chloro-3-phenyl-2H-azirine-2-carboxylate

ethyl bezoylacetate oxime

ethyl 3-oxo-3-phenylpropionate

Downstream raw materials:

3-Phenyl-6a-pyrrolidin-1-yl-1,3a,4,5,6,6a-hexahydro-cyclopenta[b]pyrrole-2-carboxylic acid ethyl ester

3-Phenyl-8a-pyrrolidin-1-yl-1,3a,4,5,6,7,8,8a-octahydro-cyclohepta[b]pyrrole-2-carboxylic acid ethyl ester

1,2,5-tricarbethoxy-3-phenyl-Δ³-1,2,4-triazoline

3-Phenyl-9a-pyrrolidin-1-yl-3a,4,5,6,7,8,9,9a-octahydro-1H-cycloocta[b]pyrrole-2-carboxylic acid ethyl ester

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