1-({2-nitrophenyl}carbonyl)-1,2,3,4-tetrahydroquinoline

Base Information

• Chemical Name: 1-({2-nitrophenyl}carbonyl)-1,2,3,4-tetrahydroquinoline
• CAS No.: 24223-25-4
• Molecular Formula: C16H14N2O3
• Molecular Weight: 282.29400
• Mol file: 24223-25-4.mol

Synonyms:1-(2-Nitro-benzoyl)-1.2.3.4-tetrahydro-chinolin;1-(2-nitro-benzoyl)-1,2,3,4-tetrahydro-quinoline;(3,4-Dihydro-2H-quinolin-1-yl)-(2-nitro-phenyl)-methanone;1-(2-Nitrobenzoyl)-1,2,3,4-tetrahydroquinoline;

Chemical Property of 1-({2-nitrophenyl}carbonyl)-1,2,3,4-tetrahydroquinoline

Chemical Property:

• Melting Point: 152 - 154 °C
• PSA: 66.13000
• LogP: 3.77600

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-({2-nitrophenyl}carbonyl)-1,2,3,4-tetrahydroquinoline

There total 3 articles about 1-({2-nitrophenyl}carbonyl)-1,2,3,4-tetrahydroquinoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,2,3,4-tetrahydroisoquinoline (635-46-1) + 2-nitrobenzyl chloride (610-14-0) → 2-[(1,2,3,4-tetrahydro-1-quinolyl)carbonyl]nitrobenzene (24223-25-4)

Guidance literature:

With triethylamine; In dichloromethane; for 1h; Ambient temperature;

DOI:10.1021/jm960133o

Reference yield:

→ 3-Methyl-1-(4-nitrobenzoyl)-1,2,3,4-tetrahydroquinoline + 2-[(1,2,3,4-tetrahydro-1-quinolyl)carbonyl]nitrobenzene (24223-25-4)

Guidance literature:

Reference yield:

→ 2-[(1,2,3,4-tetrahydro-1-quinolyl)carbonyl]nitrobenzene (24223-25-4)

Guidance literature:

1.2.3.4-Tetrahydro-chinolin, wss. NaHCO3, Ether, 2-Nitro-benzoylchlorid in Ether (20grad, 3 Std.);

upstream raw materials:

1,2,3,4-tetrahydroisoquinoline

2-nitrobenzyl chloride

Downstream raw materials:

(2-aminophenyl)(3,4-dihydroquinolin-1(2H)-yl)methanone

2-[(3,3-dimethylpiperidino)carbonyl]nitrobenzene

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