Technology Process of 2-Azidophenol
There total 6 articles about 2-Azidophenol which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
2-amino-phenol;
With
hydrogenchloride;
In
water;
at -4 ℃;
Inert atmosphere;
With
sodium nitrite;
In
water;
at 0 ℃;
for 0.166667h;
Inert atmosphere;
With
sodium azide; sodium acetate;
In
water;
at -3 ℃;
for 2h;
Inert atmosphere;
DOI:10.1007/s00775-020-01796-x
- Guidance literature:
-
With
sodium azide; copper diacetate; 1,8-diazabicyclo[5.4.0]undec-7-ene;
In
dimethyl sulfoxide;
at 95 ℃;
for 3.5h;
- Guidance literature:
-
With
copper(l) iodide; sodium azide; sodium methylate; L-proline;
In
ethanol; water;
at 95 ℃;
for 9h;
Inert atmosphere;
DOI:10.1016/j.lfs.2019.05.004
