4-chloronaphthalene-1-carbaldehyde

Base Information

• Chemical Name: 4-chloronaphthalene-1-carbaldehyde
• CAS No.: 5471-26-1
• Molecular Formula: C11H7 Cl O
• Molecular Weight: 190.63
• Hs Code.: 2913000090
• Mol file: 5471-26-1.mol

Synonyms:1-Naphthaldehyde,4-chloro- (4CI); 4-Chloro-1-naphthaldehyde;4-Chloronaphthalene-1-carboxaldehyde; NSC 26050

Chemical Property of 4-chloronaphthalene-1-carbaldehyde

Chemical Property:

• Boiling Point: 333.2°Cat760mmHg
• Flash Point: 159.7°C
• PSA: 17.07000
• Density: 1.295g/cm³
• LogP: 3.30570

Purity/Quality:

97% ^*data from raw suppliers

4-CHLORO-1-NAPHTHALDEHYDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-chloronaphthalene-1-carbaldehyde

There total 4 articles about 4-chloronaphthalene-1-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 83.0%

Dichloromethyl methyl ether (4885-02-3) + 1-Chloronaphthalene (90-13-1) → 4-chloronaphthalenecarbaldehyde (5471-26-1)

Guidance literature:

Dichloromethyl methyl ether; With tin(IV) chloride; In dichloromethane; at 0 ℃; for 0.75h;

1-Chloronaphthalene; In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/acs.orglett.0c03701

Reference yield: 55.0%

→ 4-chloronaphthalenecarbaldehyde (5471-26-1)

Guidance literature:

Reference yield:

4-chloro-1-naphthoic acid (1013-04-3) → 4-chloronaphthalenecarbaldehyde (5471-26-1)

Guidance literature:

DOI:10.1021/jo01173a003 DOI:10.1007/BF02947304

upstream raw materials:

4-chloro-1-naphthoic acid

4-chloro-1-methyl-naphthalene

Dichloromethyl methyl ether

1-Chloronaphthalene

Downstream raw materials:

(E)-3-(4-Chloro-naphthalen-1-yl)-1-(2-hydroxy-3,5-diiodo-phenyl)-propenone

4-chloro-2-naphthonitrile

4--1-naphthonitrile

[Methyl-(1-methyl-2-phenyl-ethyl)-amino]-acetic acid [1-(4-chloro-naphthalen-1-yl)-meth-(E)-ylidene]-hydrazide

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