Carbonochloridic acid, pentachlorophenyl ester

Base Information

• Chemical Name: Carbonochloridic acid, pentachlorophenyl ester
• CAS No.: 24684-80-8
• Molecular Formula: C7Cl6O2
• Molecular Weight: 328.794
• Mol file: 24684-80-8.mol

Synonyms:

Chemical Property of Carbonochloridic acid, pentachlorophenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Carbonochloridic acid, pentachlorophenyl ester

There total 2 articles about Carbonochloridic acid, pentachlorophenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

phosgene (75-44-5) + Pentachlorophenol (87-86-5,67471-28-7) → pentachlorophenyl chloroformate (24684-80-8)

Guidance literature:

With triethylamine; In tetrahydrofuran; benzene;

DOI:10.1248/cpb.15.2015

Reference yield:

→ pentachlorophenyl chloroformate (24684-80-8)

Guidance literature:

Pentachlorphenol, NaOH/COCl2;

Reference yield:

benzyloxycarbonyl-S-benzylcysteine (3257-18-9) + pentachlorophenyl chloroformate (24684-80-8) → Z-Cys(Bzl)-OPcp (13673-54-6)

Guidance literature:

Multistep reaction; (i) DMF, (ii) /BRN= 1155032/, PhNMe₂;

upstream raw materials:

phosgene

Pentachlorophenol

Downstream raw materials:

tert.-Pentyl-pentachlorphenyl-carbonat

Pentachlorphenoxycarbonyldimethyldithiocarbamat

t-butylpentachlorophenyl carbonate

2.2-Bis-<4-pentachlorphenoxy-carbonyloxy-phenyl>-propan

Refernces

• 1、 Fujino,Hatanaka. "A new reagent for the tert-butyloxycarbonylation of amino acids.". . p. 2015 - 2016. Retrieved 2007/10/05.