4--1-morpholino-7-phenylpyrido<3,4-d>pyridazine sodium salt

Base Information

• Chemical Name: 4--1-morpholino-7-phenylpyrido<3,4-d>pyridazine sodium salt
• CAS No.: 72039-43-1
• Molecular Formula: C₂₁H₂₂N₅O₄*Na
• Molecular Weight: 431.427

Synonyms:

Chemical Property of 4--1-morpholino-7-phenylpyrido<3,4-d>pyridazine sodium salt

Chemical Property:

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Technology Process of 4--1-morpholino-7-phenylpyrido<3,4-d>pyridazine sodium salt

There total 2 articles about 4--1-morpholino-7-phenylpyrido<3,4-d>pyridazine sodium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-chloro-1-morpholin-4-yl-7-phenyl-pyrido[3,4-d]pyridazine (57961-81-6) + ethanolamine (141-43-5) + bromoacetic acid methyl ester (96-32-2) → 4--1-morpholino-7-phenylpyrido<3,4-d>pyridazine sodium salt (72039-43-1)

Guidance literature:

Multistep reaction; (i), (ii) /BRN= 506256/, DMF, (iii) aq. NaHCO₃;

DOI:10.1248/cpb.27.1544

Reference yield:

1,4-dimorpholino-7-phenylpyrido[3,4-d]pyridazine (39632-88-7) → 1-morpholino-7-phenylpyrido<3,4-d>pyridazin-4(2H)-one (57961-79-2) + 4-morpholino-7-phentlpyrido<3,4-d>pyridazin-1(2H)-one (57961-78-1) + 7-(3-hydroxyphenyl)-1,4-dimorpholino-7-phenylpyrido<3,4-d>pyridazine (57696-56-7) + 7-(4-hydroxy-3-methoxyphenyl)-1,4-dimorpholino-7-phenylpyrido<3,4-d>pyridazine (72039-41-9) + 4--1-morpholino-7-phenylpyrido<3,4-d>pyridazine sodium salt (72039-43-1) + 7-(4-hydroxyphenyl)-1,4-dimorpholino-7-phenylpyrido<3,4-d>pyridazine (57696-55-6)

Guidance literature:

Product distribution; examination of metabolism in rat, dog and human; var. time,;

DOI:10.1248/cpb.28.2158

upstream raw materials:

4-chloro-1-morpholin-4-yl-7-phenyl-pyrido[3,4-d]pyridazine

ethanolamine

bromoacetic acid methyl ester

1,4-dimorpholino-7-phenylpyrido[3,4-d]pyridazine

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