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Quinoline, 2-(1-naphthalenyl)-

Base Information
  • Chemical Name:Quinoline, 2-(1-naphthalenyl)-
  • CAS No.:24702-41-8
  • Molecular Formula:C19H13N
  • Molecular Weight:255.319
  • Hs Code.:
Quinoline, 2-(1-naphthalenyl)-

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Chemical Property of Quinoline, 2-(1-naphthalenyl)-
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Technology Process of Quinoline, 2-(1-naphthalenyl)-

There total 1 articles about Quinoline, 2-(1-naphthalenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
In further solvent(s); byproducts: CO2; N2 atmosphere; refluxing in naphthalene (218°C); distribution between H2O and Et2O, addn. of NH3 to aqueous layer, extn. (Et2O), drying (MgSO4), evapn., gas chromy.;
Guidance literature:
With Na2CO3; In 2-ethoxy-ethanol; water; soln. of IrCl3*3H2O and N-ligand in 2-ethoxyethanol/H2O (3/1) refluxed for 24 h, mixt. cooled, ppt. filtered off, ppt. mixed with Na2CO3, pyrazolone derivative and 2-ethoxyethanol added, mixt. refluxed for 12 h; mixt. cooled to room temp., ppt. filtered off and chromd. (CH2Cl2/petroleum ether (2/1)); elem. anal.;
DOI:10.1021/om060037d
Guidance literature:
Multi-step reaction with 2 steps
1: water; 2-ethoxy-ethanol / 24 h / 80 °C / Inert atmosphere
2: potassium carbonate / dichloromethane / 16 h / Inert atmosphere; Reflux
With potassium carbonate; In 2-ethoxy-ethanol; dichloromethane; water;
DOI:10.1039/c8tc05263h
upstream raw materials:

{Cu(μ-O2CC6H5)(NC9H7)2}2

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